Course Structure

Introduction

All degrees are modular, with the equivalent of six modules in each year (note these may be split into sub modules). Within these modules, students will develop their skills in core chemical engineering subject matter and have the opportunity to enhance these skills through laboratory practicals, computer workshops and engineering design. Our programme is supplemented by courses in chemistry and professional development with more advanced modules in areas such as energy and materials, delivered in the later years. To obtain professional accreditation, students must follow a defined pathway.

Stage 1

Stage 1 provides you with introductory Chemical Engineering and supporting content. This introduces the principles and processes which explain how matter heats, moves and changes through different physical states or via reactions.
Stage 1 courses are outlined below:
• Fundamentals of Chemistry
• Introduction to Chemical Products and Processes
• Introduction to Engineering Design
• Maths for Chemists & Engineers
• Physical Theory
• Principles of Heat, Mass and Momentum Transfer

Stage 2

Stage 2 extends your knowledge of Chemical Engineering subject matter, building depth in the areas of thermodynamics and heat and mass transfer and providing training in the use of computational tools to design, model and control systems.
Stage 2 courses are outlined below:
• Chemical Process Thermodynamics
• Chemical Plant Design and Operation
• Fluid Mechanics
• Heat and Mass Transfer
• Process Control
• Safety and Mechanical Design

Stage 3

Stage 3 continues to add depth to core chemical engineering material and introduces new areas such as biochemical engineering. You will get to practice your skills through the design of a Chemical plant - this includes the calculation of material and energy flows, safety and environmental aspects as well as economics to demonstrate overall feasibility.
Stage 3 courses are outlined below:
• Biochemical Engineering
• Chemical Reactor Design and Process Integration
• Design Project
• Mass and Heat Transfer
• Transport Phenomena

Stage 4

Stage 4 adds both engineering depth and breadth. You will study a number of modules in advanced Chemical Engineering with specialist subjects in Sustainable and Green energy (including Photocatalytic Technologies), Design and Chemical Reaction Engineering as well as a wide-ranging options module (Advanced Topics) which includes Biopharmaceutical Engineering and Process Hazard Identification. Many of these subjects are directly linked to the internationally recognised research conducted within the school. You will also get the opportunity to not only work on a major research project with academic staff but to also develop your professional and entrepreneurial skills throughout the year.

Stage 4 courses are outlined below:

• Advanced Topics in Chemical Engineering
• Energy Systems; Oil and Gas to Renewables
• Green Chemical Engineering
• Research Project
• Environmental Engineering Design
• Advanced Chemical Reaction Engineering

Contact Teaching Hours

Medium Group Teaching

6 (hours maximum)
6 hours of practical classes or workshops each week; Design and research hours will increase as more project work is undertaken at Levels 3-4 (as applicable)

Small Group Teaching/Personal Tutorial

2 (hours maximum)
2 hours of tutorials (or later, project supervision) each week

Large Group Teaching

8 (hours maximum)
8 hours of lectures or seminars

Personal Study

24 (hours maximum)
22–24 hours studying and revising in your own time each week, including some guided study using handouts, online activities, etc.

Learning and Teaching

At Queen’s, we aim to deliver a high-quality learning environment that embeds intellectual curiosity, innovation and best practice in learning, teaching and student support to enable student to achieve their full academic potential.

On the MEng in Chemical Engineering we do this by providing a range of learning experiences which enable our students to engage with subject experts and develop attributes and perspectives that will equip them for life and work in a global society. We make use of innovative technologies and a world class library to enhance their development as independent, lifelong learners.

Examples of the opportunities provided for learning on this course are:

Design Classes

Design classes are embedded at all stages of the programme. IChemE accredited design module CHE3104 is taken at Stage 3. Significant aspects include: problem solving; sustainability, environmental awareness and safe working practices and transferable skills (such as report writing, oral presentations, IT, teamwork, critical thought, entrepreneurship).

Directed self-study

This is an essential part of life as a Queen’s student when important private reading, preparation for seminars / tutorials, writing of laboratory reports can be completed. You are encouraged to undertake private reflection on feedback, and at the later stages undertake independent research using the primary literature to support project work and critically review taught course material.

E-Learning technologies

Information associated with lectures and assignments is typically communicated via a Virtual Learning
Environment (VLE) called Canvas. Opportunities to use IT programmes associated with data manipulation and presentation are embedded in the practicals and the project- based work.

Lectures

Introduce basic information about new topics as a starting point for further directed private study/reading. Lectures also provide opportunities to ask questions, gain some feedback and advice on assessments (normally delivered in large groups to all year group peers).

Personal Tutor

Undergraduates are allocated a Personal Tutor during Level 1 and 2 who meets with them on several occasions during the year to support their academic and professional development through the discussion of selected topics.

Practicals

Laboratory practicals occur at stage 1 and stage 2 of the engineering programme. Here you will work with equipment which give you a greater understanding of the fundamental science that you will undertake within the classroom. Experiments cover areas such as heat and mass transfer, adsorption and reaction as well as many others. Our laboratory practicals are constantly updated and use modern equipment. Furthermore we train you in a number of computer software tools which will enhance your understanding and provide you with useful skills which are needed in industry.

Seminars/tutorials

Tutorials are an integral part of the programme delivery and you will undertake these within the classroom, as small groups or individually. These tutorials are designed to enhance and reinforce the learning within each module and assistance is provided by your tutors. Group work is also common throughout the programme which often requires both written submission as well as presentations. You can expect feedback on all core submitted work.

Supervised projects

Within the programme we have both research work and design with the latter embedded throughout the projects. Research projects are available within the final year only - you will work with one of the academic staff to undertake a project within a specific area, often linked to industry. Design projects occur at every year of the taught programme. Here you will work within a group under the supervision of an academic member of staff to design a chemical plant of increasing complexity and size as you progress through your degree. In the final year of the MEng programme the design aspects focus on active research areas including for example photocatalytic reactors and sustainable energy buildings - you will get the opportunity to design your own business and enhance your entrepreneurial skills. .

Assessment

Details of assessments associated with this course are outlined below:

• The way in which you are assessed will vary according to the Learning objectives of each module. Some modules are assessed solely through project work or written assignments. Others are assessed through a combination of coursework and end of semester examinations. Details of how each module is assessed are shown in the Student Handbook which is provided to all students through the VLE and on the school’s own website.

Feedback

As students progress through their course at Queen’s they will receive general and specific feedback about their work from a variety of sources including lecturers, module co-ordinators, placement supervisors, personal tutors, advisers of study and peers. University students are expected to engage with reflective practice and to use this approach to improve the quality of their work. Feedback may be provided in a variety of forms including:

• Feedback provided via formal written comments and marks relating to work that you, as an individual or as part of a group, have submitted.
• Face to face comments. This may include occasions when you make use of the lecturers’ advertised “office hours” to help you to address a specific query.
• Placement employer comments or references.
• Online or emailed comments.
• General comments or question and answer opportunities at the end of a lecture, seminar or tutorial.
• Pre-submission advice regarding the standards you should aim for and common pitfalls to avoid. In some instances, this may be provided in the form of model answers or exemplars which you can review in your own time.
• Feedback and outcomes from practical classes.
• Comments and guidance provided by staff from specialist support services such as, Careers, Employability and Skills or the Learning Development Service.
• Once you have reviewed your feedback, you will be encouraged to identify and implement further improvements to the quality of your work.

Modules

• Year 1

  Core Modules

  Introductory Mathematics for Chemists and Engineers (10 credits)

  ×

  Introductory Mathematics for Chemists and Engineers

  Overview

  STAFF
  
  NAME CONTRIBUTION
  Dr L. Stella
  l.stella@qub.ac.uk Weeks 1-5: Lectures (10 hrs); Tutorials (10 hrs).
  Dr B. Xiao
  b.xiao@qub.ac.uk Weeks 9-12: Lectures (8 hrs); Tutorials (8 hrs).
  Dr M. Huang
  m.huang@qub.ac.uk Weeks 6-8: Lectures (6 hrs); Tutorials (6 hrs).
  Demonstrators Tutorials (22 hrs)
  
  
  Detailed Syllabus – Lectures (26 Hours):
  Note: The following topics may be slightly rescheduled to meet the class requirements or due to unforeseen contingencies.
  
   Week 1: Foundation maths (2 hrs, only for non A-level Maths students)
  Why Maths? Numbers (integers, decimals, significant figures, scientific notation); Formula and algebraic manipulations; Role of units.
   Week 2: Introduction (2 hrs):
  Representing chemical data; linear dependence; equation of the line; interpolation; parabolic behaviour; inverse proportionality (hyperbolic behaviour); Cartesian representation of a function (analytic geometry); Implicit representation (circle, ellipse).
   Week 3: Basic Functions I (2 hrs):
  Polynomials; the parabola again; intersects and solution of second order equation; higher order equation; factorisation of polynomials; rational functions; singular points; drawing a rational function (the concept of limit); simplification of rational functions.
   Week 4: Basic Functions II (2 hrs):
  Circular functions (trigonometry); drawing circular functions (periodicity); waves; trigonometric identities; inverse functions; power laws; properties of powers; rational exponent; drawing power laws (rate of growth);
   Week 5: Basic Functions III (2 hrs):
  Real exponents (rational approximation); the exponential function; properties of the exponential; the logarithmic function (inverse of the exponential); properties of the logarithms; hyperbolic functions (link with the exponential function).
   Week 6: Differentiation I (2 hrs):
  Local behaviour of functions; finding the tangent line; definition of the derivative; derivatives polynomials and simple functions; Newton's method to find the roots of an equation; higher derivatives.
   Week 7: Differentiation II (2 hrs):
  Differentiation rules; derivatives of rational function; differentiation of complicated expressions (tricks); partial differentiation; differentiation of implicit functions (thermodynamic applications).
   Week 8: Differentiation III (2 hrs):
  Geometric application of the derivatives; minima and maxima; inflection points;
   Week 9: Integration I (2 hrs):
  The problem of measuring area; thermodynamic examples; the construction of the integral (Riemann); integration as the inverse of differentiation; simple integrals; improper integrals.
   Week 10: Integration II (2 hrs):
  Integration rules (by parts, by change of variables); Integrations of common functions (tricks); Integration of the solid of revolution.
   Week 11: Integration III (2 hrs):
  Integrals that cannot be computed analytically; numerical integration (trapezium and Simpson rules); analysis of the errors.
   Week 12: Complex numbers (2 hrs):
  Why complex numbers? the imaginary unit; the fundamental theorem of algebra; Adding and multiplying complex numbers; the complex conjugate; dividing complex numbers; polar representation; De Moivre's formula; complex exponential; Euler's formula; links to the circular functions.
  
   TUTORIALS (22 hours):
  Note: The following topics may be slightly rescheduled to meet the class requirements or due to unforeseen contingencies.
  
   Week 1: Foundation maths (2 hrs)
   Week 2: Introduction (2 hrs)
   Week 3: Basic functions I (2 hrs)
   Week 4: Basic functions II (2 hrs) – CANVAS Quiz (20%)
   Week 5: Basic functions III (2 hrs)
   Week 6: Differentiation I (2 hrs)
   Week 7: Differentiation II (2 hrs)
   Week 8: Differentiation III (2 hrs) – CANVAS Quiz (20%)
   Week 9: Integration I (2 hrs)
   Week 10: Integration II (2 hrs)
   Week 11: Integration III (2 hrs
   Week 12: Complex numbers (2 hrs) – CANVAS Quiz (20%)
   Week 13: Class test (40%)

  Learning Outcomes

  LEARNING OUTCOMES:
  At the end of the module, students will be able to:
  • Recognize and manipulate an appropriate range of mathematical tools required in chemistry and chemical engineering.
  • Demonstrate the application of mathematics to solve routine chemistry and chemical engineering problems.
  • Model simple chemistry and chemical engineering processes.
  
  In particular, students will be able to solve problems involving:
  • Polynomials and elementary functions
  • Cartesian representation of functions
  • Numerical solution of nonlinear equations
  • Differentiation and its applications
  • Integration and its applications
  • Complex numbers

  Skills

  SKILLS ACQUIRED:
  Students will grow their confidence in identifying and applying mathematical tools required to progress their studies in either chemistry or chemical engineering. During the module, students will practice:
  • Logical thinking
  • Critical assessment of a mathematical derivation
  • Independent and group learning

  Coursework

  100%

  Examination

  0%

  Practical

  0%

  Credits

  10

  Module Code

  CHE1107

  Teaching Period

  Autumn

  Duration

  12 weeks

  Pre-requisite

  No

  Core/Optional

  Core

  Physical Theory (30 credits)

  ×

  Physical Theory

  Overview

  STAFF
  
  NAME CONTRIBUTION
  Dr A. Doherty
  A.P.Doherty@qub.ac.uk Kinetics (6 hours lectures, 2 hours seminars)
  Electrochemistry (5 hours lectures, 1 hour seminar and 1 tutorial)
  Dr M. Huang
  m.huang@qub.ac.uk Laboratory Classes
  Dr P. Kavanagh
  p.kavanagh@qub.ac.uk Phase Equilibria, (10 hours lectures, 3 hours seminars, 2 hours assessment); Laboratory Classes
  Dr L. Moura
  l.moura@qub.ac.uk Basic Thermodynamics, (8 hours lectures, 4 hours seminars and 1 tutorial)
  Dr L. Stella
  l.stella@qub.ac.uk Computer Workshops (6 hours)
  Dr J. Thompson
  jillian.thompson@qub.ac.uk Chemical Equilibria (10 hours lectures, 3 hours seminars); Laboratory Classes
  Dr J. Vyle
  j.vyle@qub.ac.uk Physical Chemistry Aspects of Drug Design (6 hours lectures, 3 hours seminars and 1 tutorial)
  
  Lecture content
  Chemical Equilibria (10 hours lectures, 3 hours seminars):
   1.1 Introduction to physical chemistry: review states of matter and introduction to ideal gases and ideal solutions, enthalpy and internal energy, Hess cycles, heat capacity and heat transfer.
   1.2 Chemical Equilibria: Definitions and calculations involving equilibrium constants Kc and Kp, including examples of homogeneous and heterogeneous equilibria (Ksp). Definitions and calculations involving enthalpy of solution and lattice energy. Application of Le Chatelier’s Principle to determine the effect of change in concentration, pressure, temperature and catalyst on the composition of the reaction mixture and the equilibrium constant. The Common Ion Effect.
   1.3 Acids and Bases: Definitions of conjugate acid and base; strong and weak acids and bases. Calculation of pH, pKa and pKb. The special case of water Kw and pKw Terminology in acid/base titrations, calculation of pH at the end point, and indicators. Definition of a buffered solution and calculation of its pH. Examples of polyfunctional acids and their behaviour in titrations.
  
  Phase Equilibria (10 hours lectures, 3 hours seminars, 2 hours class test – first semester):
   2.1. Phase Change: Phase changes including melting temperature, boiling temperature, density and molar volume, lattice energy, bond dissociation energy, enthalpy of vaporisation, introduction to entropy.
   2.2. One Component Systems: Phase equilibria in single component systems using simple
  P-T diagrams, the phase rule. Vapour pressure – temperature relationships: the Clapeyron and Clausius-Clapeyron Equations, the Antoine Equation.
   2.3. Two-component systems (vapour-liquid equilibria of ideal systems): Raoult’s Law, Dalton’s Law and Henry’s Law applied to ideal two component systems, volatility and relative volatility, constant pressure diagrams (x,y and T-x,y) and the Lever rule.
   2.4. Introduction to non-ideal solutions: An azeotrope being a mixture that vaporizes and condenses without a change in composition; a eutectic being a mixture that freezes and melts without change of composition.
   2.5. Colligative properties: Relative lowering of vapour pressure, boiling point elevation and boiling point depression in binary solutions containing non-volatile solutes; osmotic pressure.
  
  Kinetics (6 hours lectures, 2 hours seminars):
   3.1. Key concepts: Elementary reactions, reaction molecularity, molecularity vs. stoichiometry, definition of reaction rates, calculating reaction rates from experimental data, writing differential rate laws, reaction orders, order vs. molecularity, reaction rate constants, initial rates method, integrated rate laws (how and why), collision and transition state theories, Arrhenius rate law and activation energy, reaction kinetics in relation to reaction mechanism. Catalysis. Methods of measuring reaction rates.
   3.2. Derivation of rate equations: Derivation of zero, 1st and 2nd rate laws, experimental data analysis and visualisation, Obtaining reaction orders and rate constants by the initial rates method. Analysing data using integrated rate laws and making predictions.
   3.3. Collision and transition state theories: The Arrhenius equation. Activation by collision and the collision theory. Measurement of activation energies.
   3.4. Classes of reaction: Simple gas phase reactions. Chain and branched chain reactions. Reactions in solution, reactions of solids, catalysed reactions.
  
  Basic Thermodynamics, (8 hours lectures, 4 hours seminars and 1 tutorial):
   4.1. Summary review. Thermodynamics and the concepts of temperature, heat/energy flow and thermal equilibrium. Introduction to enthalpy, work, internal energy, zeroth law of thermodynamics, the first law of thermodynamics, state function, standard conditions, enthalpy of formation.
   4.2. The direction of spontaneous change. Spontaneous vs non-spontaneous change. Entropy as criterion for spontaneous change. Reversible and irreversible processes. Classical and molecular basis of entropy.
   4.3. The second law of thermodynamics. Examples and calculations using standard entropies; entropy changes with volume, temperature, phase transitions and chemical reactions.
   4.4. Absolute entropy and the third law of thermodynamics.
   4.5. Chemical equilibrium: Gibbs energy and spontaneity, energy minimum, direction of chemical change and influence of enthalpy and entropy. Variation of Gibbs energy with temperature, pressure and concentration. Gibbs energy relationship with equilibrium and the equilibrium constant. Examples and calculations.
   4.6. Gibbs energy and phase equilibria. The thermodynamics of transition. Review of one component and two component phase diagrams. Liquid-liquid equilibria, phase separation, critical solution temperature, distillation of partially miscible liquids. Examples of extractions, separations and molecular interactions.
  
  Electrochemistry (5 hours lectures, 1 hour seminar and 1 tutorial) :
   5.1. Introduction to Electrochemistry: Equilibrium vs. Dynamic Electrochemistry classification; Units / dimensions electronic charge, coulombs; Review of Faraday’s Law; What is an electrode? Redox reactions at electrodes; Charge separation at interfaces and interfacial electric potential; Spontaneous vs. non-spontaneous charge separation; “Kinds” of electrodes; Electrode potentials = ΔG / -nF; Nernst equations for different “kinds” of electrodes; Effects of temperature and concentration on electrode potentials; Importance of the Standard Hydrogen Electrode.
   5.2 Electrochemical Cells: Electrochemical series; Electrochemical cells, net cell reactions, cell diagrams; Calculating cell potentials, ΔG overall and K, equilibrium constant; Calculating solubility of salts from cell potential measurements; Calculating cell potentials from thermodynamic data; H2/O2 fuel cell description / performance; Cell thermodynamics, potentials vs. ΔS (entropy changes) relationship.
  
  Physical Chemistry Aspects of Drug Design (6 hours lectures, 3 hours seminars and 1 tutorial):
   6.1 Introduction to the physical properties of drugs and their targets: Recognising hydrogen bond donors and acceptors in biomolecules and in API’s (especially β-lactam antibiotics); binding affinities and selectivity; screening potential drug molecules using Lipinski’s Rule; prodrug activation strategies.
   6.2 Basic Pharmacodynamics and Pharmacokinetics: Quantitative dose response curves and rates of elimination.
  
  Laboratory Classes (21 hours):
   Students will be divided into groups. Each group will carry out 7 different experiments (3 hrs each):
   P1 The Catalysed Decomposition of Hydrogen Peroxide in Aqueous Solution;
   P2 Buffers and pH Measurement;
   P3 Phase Transfer and Solubility of I3-;
   P4 Concentration Cells and Electrode Potentials;
   P5 Enthalpy and Entropy of Vaporisation;
   P6 Determination of the Activation Energy of a Reaction;
   P7 Visualisation of 3D structure of a medicinal chemistry compound.
   Both an individual COSHH assessment and pre-lab assessment as well as an individual post-lab report will be submitted for each experiment as indicated on Canvas.
  
  Computer Workshops (6 hours):
   Students will attend two computer-based workshops
   Using Excel for calculation and graphing
   Using Excel for statistical analysis

  Learning Outcomes

  On completion of this module a learner should be able to:
   Explain and use equations to describe chemical systems at equilibrium.
   Describe the general principles of phase equilibria as applied to single and binary component systems.
   Understand and apply the basic rules of chemical kinetics.
   Describe and apply the general principles of the first and second laws of thermodynamics.
   Describe equilibria of electrochemical cells and discuss applications of electrochemical theory.
   Explain the chemistry of drug design and interaction.
   Improved practical skills:
   General chemical and engineering laboratory skills including estimation of experimental error.
   Increased awareness of laboratory health and safety requirements.
   Use of Excel for calculations and graphing.
   Use of ChemDraw for presentation of chemical structures.
   Gained transferrable skills:
   Basic thermodynamic, kinetic and electrochemistry knowledge, basic laboratory skills, use of ChemDraw, Excel and estimation of error in experimental results.

  Skills

  Skills associated with module:
  Thermodynamic and kinetic problem solving (including numerical), Excel-based calculations, graphing. General chemical and engineering laboratory skills including statistical analysis.
  In addition,
  Communication – spoken during practicals, tutorials and seminars and written in lab reports, tutorials, class tests and exam.
  Numeracy – basic algebra and calculus.
  Improved independent learning and time management.
  Problem-solving –solving problems in exams, tutorials, seminars and practicals.
  Safe handling of chemical materials, taking into account their physical and chemical properties, including any specific hazards associated with their use. Accurate measurement and recording of data and appreciation of error.
  Standard laboratory procedures involved in physical chemistry.

  Coursework

  15%

  Examination

  60%

  Practical

  25%

  Credits

  30

  Module Code

  CCE1102

  Teaching Period

  Both

  Duration

  24 weeks

  Pre-requisite

  No

  Core/Optional

  Core

  Mathematics for Chemical Engineers (10 credits)

  ×

  Mathematics for Chemical Engineers

  Overview

  STAFF
  
  NAME CONTRIBUTION
  Dr L. Stella
  l.stella@qub.ac.uk Weeks 16-18: Lectures (6 hrs); Tutorials (6 hrs).
  Weeks 24-25: Lectures (4 hrs); Tutorials (4 hrs).
  Dr Kevin Morgan
  k.morgan@qub.ac.uk Weeks 14-15: Lectures (4 hrs); Tutorials (4 hrs).
  Weeks 20-23: Lectures (8 hrs); Tutorials (8 hrs).
  Demonstrators Tutorials (46 hrs)
  
  
  Detailed Syllabus –– Lectures (22 Hours):
  
  Note: The following topics may be slightly rescheduled to meet the class requirements or due to unforeseen contingencies.
  
   Week 17: Matrices I (2 hrs):
  Addition, subtraction, multiplication by scalar, matrix multiplication, transpose, special matrices, determinant of 2×2 matrix.
  
   Week 18: Matrices II (2 hrs):
  Minors, cofactors, determinant of 3×3 matrix, properties of determinants. Set of linear equations written in matrix form, Cramer’s rule, adjoint and inverse of a square matrix.
  
   Week 19: Vectors I (2 hrs):
  Magnitude, unit vector, position vector, line segment theorem, components. Scalar product, applications of scalar product (angle between vectors, work done, component of vector, projections).
  
   Week 20: Vectors II (2 hrs):
  Vector product, applications of vector product (area of triangle, perpendicular direction, moment of force). Vector kinematics.
  
   Week 21: Maclaurin and Taylor series (2 hrs):
  Maclaurin series of elementary functions; Taylor series; Power series of complicated expressions (tricks).
  
   Week 22: Reading week, no lecture.
  
   Week 23: Differential equations I (2 hrs):
  Classification, modelling of physical problems. Analytical solution of first order differential equations. Direct integration, general and particular solutions, boundary, and initial
  
   Week 24: Differential equations II (2 hrs):
  Variables separable equations. Linear equations.
  
   Week 25: Differential equations III (2 hrs):
  Numerical solution of first order initial value problem using Euler’s method. Solution of second order differential equations, simple integration.
  
   Week 26: Differential equations IV (2 hrs):
  Second order linear differential equations with constant coefficients, complementary function. Particular integral.
  
   Week 27: Laplace transforms I (2 hrs):
  Definition, table for common functions, inverse Laplace transform.
  
   Week 28: Laplace transforms II (2 hrs):
  Application to solution of differential equations.
  
  TUTORIALS (22 hours):
   Note: The following topics may be slightly rescheduled to meet the class requirements or due to unforeseen contingencies.
  
   Week 17: Matrices I (2 hrs)
   Week 18: Matrices II (2 hrs)
   Week 19: Vectors I (2 hrs) – CANVAS quiz (10%)
   Week 20: Vectors II (2 hrs)
   Week 21: Maclaurin and Taylor series (2 hrs)
   Week 22: Reading week, no tutorial.
   Week 23: Differential equations I (2 hrs)
   Week 24: Differential equations II (2 hrs) – CANVAS quiz (10%)
   Week 25: Differential equations III (2 hrs)
   Week 26: Differential equation IV (2 hrs)
   Week 27: Laplace transforms I (2 hrs)
   Week 28: Laplace transforms II (2 hrs) – CANVAS quiz (10%)
   Week 29: Class test (20%)

  Learning Outcomes

  On completion of this module a learner should be able to:
   Recognize and manipulate an appropriate range of mathematical tools required in chemistry and chemical engineering.
   Demonstrate the application of mathematics to solve routine chemistry and chemical engineering problems.
   Model simple chemistry and chemical engineering processes.
   In particular, students will be able to solve problems involving:
   Vectors and matrices
   Ordinary differential equations
   Laplace transform
   Basic statistics

  Skills

  Learners are expected to demonstrate the following on completion of the module:
   Students will grow their confidence in identifying and applying mathematical tools required to progress their studies in either chemistry or chemical engineering. During the module, students will practice:
   Logical thinking
   Critical assessment of a mathematical derivation
   Independent and group learning

  Coursework

  100%

  Examination

  0%

  Practical

  0%

  Credits

  10

  Module Code

  CHE1108

  Teaching Period

  Spring

  Duration

  12 weeks

  Pre-requisite

  No

  Core/Optional

  Core

  Introduction to Chemical Products and Processes (20 credits)

  ×

  Introduction to Chemical Products and Processes

  Overview

  STAFF
  
  NAME CONTRIBUTION
  Dr Robin Curry
  r.curry@qub.ac.uk
  3 Lectures (6. Energy generation; 7. Introduction to unit operation processes)
  2 Workshops (Energy generation)
  Dr Nicole Gui module co-ordinator
  m.gui@qub.ac.uk
  6 Lectures – 1. Introduction to Chemical Industry; 4. Materials and Energy Balances;
  15 Workshops – 2. Materials and Energy balances; 5.3; 5.5; 5.7.
  Dr Patricia Marr
  p.marr@qub.ac.uk
  6 Lectures (3. Principles of green and sustainable chemistry)
  2 Workshops (Sustainable chemistry)
  Dr Kevin Morgan
  k.morgan@qub.ac.uk
  6 Lectures ¬– 2. Unit Conversion and Dimensional Analysis; 5. Introduction to Chemical Manufacturing Processes (5.1, 5.2, 5.4; 5.6)
  5 Workshops – Units conversion and dimensional analysis; Case studies of industrial processing and manufacturing.
  
  Detailed Syllabus – Lectures/Tutorials (21 hours/24 hours):
   1. Introduction to Chemical Industry (Lec. 2 hrs.) Dr N. Gui
   1.1. Introduction to chemical industry. 1.2. Background and development of the Chemical Industry. 1.3. The future of chemical industry. 1.4. Introduction to sustainable processing.
  
   2. Unit Conversion & Dimensional Analysis (Lec. 2 hrs. Work. 2 hrs.) Dr K. Morgan
   2.1. System of units and unit conversion. 2.2 Physical properties. 2.3. Dimensional analysis. 2.4. Dimensionless groups.
  
   3. Principles of Green & Sustainable Chemistry (Lec. 6 hrs. Work. 2 hrs.) Dr P. Marr
   3.1. Principles of Green Chemistry. 3.2. Examples of green and sustainable Chemistry in practice.
  
   4. Material and Energy Balances Dr N. Gui
   4.1. Material balances: (Lec. 2 hrs. Work. 4 hrs.)
  -single unit and multiple unit systems under steady state condition.
  -Material balance for steady-state reaction system.
   4.2. Energy balances: (Lec. 2 hrs. Work. 4 hrs.)
  -single unit and multiple unit system under steady state condition.
  -energy balance for steady state reaction system.
   4.3. Steam tables (Work. 4 hrs.)
  
   5. Introduction to Chemical Manufacturing Processes (Lec. 4 hrs. Work. 6 hrs.)
   5.1. Introduction to product and process design. 5.2. Strategies of product and process design. 5.3. Flow diagrams. 5.4. Environmental and safety considerations. 5.5. Waste reduction and resource management. 5.6. Risk assessment. 5.7. Reporting design data. 5.8. Case studies of industrial manufacturing processes: process, applications, and environment pollution (workshops)
  
   6. Energy generation (Lec. 3 hrs. Work. 2 hrs) Dr R. Curry
   6.1. Introduction. 6.2. Renewable energy generation. 6.3. Bioenergy system.
  
  
  Renewable Energy Generation – Group projects:
   For renewable energy generation, students will be divided into small groups and given a consultancy brief to provide advice to a locally-based company on an outline design of a Gasifier Plant, to provide renewable energy for their manufacturing facility. Each group must review the range of gasifier designs currently in operation and based on this review, to produce a final report with recommendations for the most suitable design choice, to be submitted for assessment at the end of the semester.

  Learning Outcomes

  On completion of this module a learner should be able to:
   Understand the essential professional requirements of the chemical industry
   Understand the idea of sustainable processing in the chemical industry.
   Understand the role of chemistry in modifying chemical properties.
   Explain key factors in chemical product design and development.
   Describe key physical properties of materials.
   Demonstrate knowledge of unit conversion and dimensional analysis techniques relevant to chemistry/chemical engineering calculations.
   Discuss the principles of green chemistry.
   Understand the principles of material and energy balances
   Apply the principles of materials and energy balances in solving problems related to chemical processes.
   Understand relevant elements associated with chemical engineering, such as renewable energy generation and bioenergy system.
   Produce simple process flow diagrams based on written process descriptions.
   Describe the ethical principles related to the chemical industry and the consequences of unethical practices.
   Demonstrate an understanding of the importance of health, safety and environmental management in the chemical process industry.

  Skills

  Skills associated with module:
   STEM – Core skills in underlying physics, chemistry and maths and biology are applied to solving problems including dimensional analysis, mass and energy balances, efficiency calculation and economic evaluation.
   Independent and team working - Group and individual assessments.
   Analytical – Evaluation of data and its use in design.
   Communication – discussion of important factors in the chemical industry and the presentation of data including written reports.
   Learning and management - Improving time management.

  Coursework

  100%

  Examination

  0%

  Practical

  0%

  Credits

  20

  Module Code

  CHE1101

  Teaching Period

  Autumn

  Duration

  12 weeks

  Pre-requisite

  No

  Core/Optional

  Core

  Introduction to Engineering Design (10 credits)

  ×

  Introduction to Engineering Design

  Overview

  Staff
  Name and contribution
  Dr Robin Curry
  r.curry@qub.ac.uk
  3 Lectures – Introduction to Unit Operation Processes
  
  Dr Nicole Gui (module co-ordinator)
  m.gui@qub.ac.uk
  20 Workshops - Design project
  
  Dr Kevin Morgan
  k.morgan@qub.ac.uk
  4 Workshops - CHP tour
  
  Dr Chunfei Wu
  c.wu@qub.ac.uk
  6 Seminars - (Aspen computer lab)
  
  Detailed Syllabus – Lectures/Tutorials (3 hours):
  
  1. Introduction to Unit Operation Processes - Dr R. Curry
  1.1. Basic fluid transfer equipment: mixers, pumps, valves, compressor, turbine.
  1.2. Heat transfer equipment: heat exchangers, design and operation.
  1.3. Mass transfer equipment: distillation, solvent extraction, filtration, absorption units.
  1.4. General concept of operation: batch and continuous, heating/cooling system, flow arrangement.
  
  Details of Workshops/Seminars (30 hours):
  
  The seminar sessions will focus on creative problem solving and guidance towards completion of design project.
  
  1. CHP tour (Dr K. Morgan) 4 hours
  2. Aspen (computer lab, Dr C. Wu) 6 hours
  3. Design project (Dr N.Gui) 20 hours
  
  
  Design Project – Group projects:
  Students will be divided into group of five and will be given a specific design statement. Each group of students will be asked to produce a process design based on their design statement and perform mass and energy balance calculations, as well as basic design calculations for the process. The students are also expected to design simple unit operations such as pumps and heat exchangers with the guidance given. Lastly, a final report compiling the calculated data and detail analysis of operating conditions will be submitted at the end of the semester. Peer review assessment will be conducted as a measure of the group working performance of each individual student.

  Learning Outcomes

  On completion of this module a learner should be able to:
  Use computer aid software, Aspen to obtain physical properties of chemical components and perform simple process simulation.
  Apply the knowledge gained from other modules in chemical process design.
  Design simple process equipment for specified operating conditions provided.
  Describe the basic key features, operation modes and condition of industrial equipment.
  Develop important time management skills and group work as well as able to meet both group and individual project deadlines.
  Demonstrate an ability to analyse uncertainties in design and perform critical thinking.
  Develop literature review and design report writing skills.

  Skills

  Learners are expected to demonstrate the following on completion of the module:
  Analytical and computational skill – Use of Excel for calculations and graphing.
  Problem solving skill – Completing design problems centered on individual unit operations and on a small process.
  Creative thinking – Enhanced through development of operating strategies to increase process efficiency.
  Communication skills – Reporting of design information, calculated data with critical analysis of the design data.
  Moral and ethical reasoning.
  Learning and management – effective time management to complete the assignment within scheduled timeline.

  Coursework

  100%

  Examination

  0%

  Practical

  0%

  Credits

  10

  Module Code

  CHE1105

  Teaching Period

  Spring

  Duration

  12 weeks

  Pre-requisite

  No

  Core/Optional

  Core

  Principles of Heat, Mass and Momentum Transfer (20 credits)

  ×

  Principles of Heat, Mass and Momentum Transfer

  Overview

  STAFF
  
  NAME CONTRIBUTION
  Dr D. Poulidi,
  d.poulidi@qub.ac.uk. Basics of Heat and Mass Transfer (15 hours); Fluid Flow (15 hours); Basics of heat and mass transfer (4 hours - 2 assessed tutorials);
  Fluid flow (2 hours - 1 assessed tutorial); Lab Briefing (1 hour);
  Dr J. Thompson,
  jillian.thompson@qub.ac.uk. Separation Processes (18 hours); Separation Processes (2 hours - 1 assessed tutorial);
  Dr K. Morgan
  k.morgan@qub.ac.uk Practical Classes.
  Mrs S. Evans Practical Classes.
  The hours allocated here include problem classes as required per section.
  
  Basics of Heat and Mass Transfer (13 hours):
   1.1. Introduction to transport phenomena;
   1.2. Links between heat, mass and momentum transport.
   1.3. Introduction to mass transfer;
   1.4. Molecular and convective diffusion – Fick’s law;
   1.5. Unimolecular diffusion;Equimolar counter diffusion; Non-equimolar counter diffusion;
   1.8. Liquid-liquid diffusion.
   1.9. Basics of heat transfers by conduction and convection;
   1.10. Thermal resistance networks;
   1.11. Critical and economic thickness of insulation;
   1.13. Heat generation from solids;
   1.14. Heat exchanger design (Condensers, vaporisers, multipass exchangers).
  
  Fluid Flow (12 hours):
   2.1. Properties of fluids, units and dimensions.
   2.2. Fluid statics (Pascal’s law and its applications).
   2.3. Fluid dynamics (Bernoulli equation).
   2.4. Energy and momentum equations and their applications.
   2.5. Incompressible flow in pipes.
   2.6. Fluid flow measurements.
   2.7. Pumps.
  
  Separation Processes (18 hours):
   3.1. Solvent extraction: 10 hours:
   3.1.1. Introduction to separations;
   3.1.2. Introduction to LLE and binodal curves including tie-lines and the Lever Rule;
   3.1.3. Distribution coefficients, plotting and using ternary diagrams;
   3.1.4. Use of ternary diagrams for solvent extraction.
   3.1.5. Seminar on solvent extraction problem.
   3.2 Distillation: 8 hours:
   3.2.1. Introduction to single and multiple flash separations;
   3.2.2. Introduction of the McCabe-Thiele method for distillation and use of mass balances to derive equations for the ROL, SOL and q-line;
   3.2.3. The reflux ratio, cases of total and minimum reflux and the Fenske Equation, calculation of q-lines for sub-cooled and super-heated liquids;
   3.2.4. Worked example of all aspects of McCabe Thiele method from use of Antoine Equation or dePriester charts to determine the phase equilibria data through to determination of the number of stages at total reflux, the minimum reflux ratio as well as the number of stages and optimum feed location at a multiple of the minimum reflux ratio, introduction to efficiencies.
  
  Class test (2 x2 Hours):
   Class tests constitute part of the continual assessment.
   Two 2-hour tutorials (a total) of the module mark each will take place during the module (as shown below). The content of the class tests will be communicated in class
  
  Labs (9 hours):
  
   Lab Briefing (1 hour):
  A lecture will be given to introduce the students to the laboratory elements of the module.
   Practical Classes:
   Students will be divided into groups. Each group will carry out 3 different experiments:
   Shell and tube heat exchanger (3 hours).
   Fluid flow (3 hours).
   Vapour liquid equilibria (3 hours).
   Both an individual pre-lab report and an individual report will be submitted for each experiment as indicated in the lab manual (to be handed out in the beginning of the term).

  Learning Outcomes

  Learning outcomes:
  By the end of the module, the students will be able to:
  • perform fluid flow measurement calculations;
  • apply mass and energy balance equations of fluids in motion;
  • apply the Bernoulli equation in order to calculate pressure drops and velocities in pipe measurements;
  • describe basic pump and valve designs;
  • perform basic heat transfer calculations for heat transfer by conduction and convection;
  • produce a thermal resistance network for mixed heat transfer and calculate individual and total resistances and heat transfer rates;
  • design a basic heat exchanger (condensers, vaporisers, multipass exchangers);
  • obtain maximum and surface temperature in the case of heat generation in solids
  • determine concentration profiles in mass transfer by diffusion;
  • describe different separation units in the chemical industry and discuss their relevance for different applications;
  • gain an appreciation of binary and ternary liquid phase extraction processes;
  • present ternary data in graph form and apply this to obtain solvent extraction mass balances;
  • use mass and component balances to derive equations for the operating lines in a binary mixture distillation column and use these to apply the McCabe-Thiele method to design a distillation column.

  Skills

  Learners are expected to demonstrate the following on completion of the module:
   The students will gain the necessary theoretical background that will allow them to carry out a design of basic unit operations.
   In addition, through participation in lab and tutorial classes the students will be able to interpret and synthesise information presented in class and produce a summarised version of key points. They will also acquire skills in problem solving at tutorials, report writing through lab reports, communication in lab classes, lectures and tutorials and time management.

  Coursework

  35%

  Examination

  50%

  Practical

  15%

  Credits

  20

  Module Code

  CHE1103

  Teaching Period

  Spring

  Duration

  12 weeks

  Pre-requisite

  No

  Core/Optional

  Core

  Fundamentals of Chemistry (20 credits)

  ×

  Fundamentals of Chemistry

  Overview

  STAFF
  
  NAME CONTRIBUTION
  
  Dr A. C. Marr a.marr@qub.ac.uk
  Module Co-ordinator
  General Chemistry - 18 Lectures; Skills Workshops – part 1, Essential Calculations for Practical Chemistry
  Dr P. C. Marr p.marr@qub.ac.uk
  Skills workshop – Laboratory Skills parts 1 and 2
  Prof. P. Stevenson p.stevenson@qub.ac.uk
  Organic Chemistry: Functional Group Chemistry 15 Lectures, 5 Seminars Organic Chemistry Laboratory
  Dr P. Dingwall p.dingwall@qub.ac.uk
  Organic Chemistry Laboratory
  Dr M. Swadzba-Kwasny Swadzba-kwasny@qub.ac.uk
  Skills workshop – Scientific writing and researching skills.
  
  Course content
  
  General Chemistry - Elements, Atoms, ions, electrons and the periodic table. This course aims to give an introduction to the fundamental principles of atoms from the chemists’ viewpoint. Starting from a simple model and using the results of quantum mechanics a more appropriate model of the atom is presented. From this model trends in atomic and ionic properties which enable us to explain differences and similarities and predict the properties of different elements can be deduced. The following topics are covered:
  * The Basics: Element, The periodic table, atom, mole.
  * The Atom: The Bohr Atom.
  * The Electron: Wave-Particle Duality and The Schrödinger Wave Equation, Probability Density, Radial Distribution Function, Orbitals, Quantum Numbers, s and p Orbitals, Phase, d Orbitals.
  * More than One Electron: Filling orbitals, The aufbau principle, The Pauli Exclusion Principle, Hund’s rules, Penetration, Shielding, Effective Nuclear Charge, Slater’s Rules, Size.
  * Trends: Ionization energy, Electron attachment enthalpy (affinity), Electronegativity, Ionic radii, Polarizability and polarizing power, Hydration enthalpies, Redox potentials. General Chemistry - Structure and Bonding. This course introduces some important theories of bonding. Theories of bonding are discussed in some detail for discrete molecules. The discussion of bonding in molecular species centres on the valence bond and molecular orbital theories. Intermolecular forces between molecules are also discussed.
  * Introduction to bonding: Discussion of types of structure and common bonding theories, examples of representative structures.
  * Homonuclear Diatomic Molecules: Interatomic distance and covalent radii, Potential energy curves, attractive and repulsive forces, bond energy and enthalpy. Lewis structures, filled shells, the octet rule. Wavefunction, introduction to valence bond theory and molecular orbital theory, Valence bond theory: ionic and covalent contributions, resonance; Molecular orbital theory: molecular orbitals, linear combinations of atomic orbitals, orbital overlap, bonding and antibonding orbitals, MO diagrams, some shapes of MO’s, labelling MO’s, examples of simple MO diagrams, bond order.
  * Heteronuclear Diatomic Molecules: Lewis structures, valence bond approach, Molecular orbital theory, energy matching, symmetry, non-bonding orbitals; electronegativity, electric dipole moments, carbon monoxide, isoelectronic molecules.
  * Polyatomic Molecules: Metal complexes and covalent polyatomics, coordination number, common geometries, molecules obeying the octet rule, valence bond theory, expanding the octet, hybridization (sp, sp2, sp3), formal charge, single, double and triple carbon-carbon bonds, molecular shapes; molecular orbital theory: ligand group orbitals; comparison of VB and MO, macromolecules, fullerenes, proteins and hydrogen bonding.
  * Intermolecular Forces: Van-der-Waal forces, strength of forces.
  * Introduction to solids with extended structures: metals and semi-metals, ionic solids and covalent solids. Only covered if time permits. ORGANIC CHEMISTRY: Functional Group Chemistry
  * Draw structural formula to represent organic compounds, identify isomers and convert structural formula to molecular formula.
  * Identify common organic functional groups, name organic compounds containing these groups, and predict their chemistry and reactivity.
  * Recognise nucleophiles, electrophiles and bases and identify which chemistry these species participate in. Appreciate the importance of acidity and basicity in organic chemistry
  * Sketch substitution, elimination and addition mechanisms and appreciate the importance of ‘mechanism’ in rationalising organic chemical reactions. * Suggest reagents for interconverting one functional group into another. * The functional groups which will be used to illuminate these outcomes are alkanes, alcohols, amines, alkyl halides, alkenes, alkynes, carbonyls compounds including aldehydes, ketones, carboxylic acids, esters and amides.
  SKILLS WORKSHOPS:
  * Scientific writing and researching skills
  * Laboratory skills
  * Essential calculations for practical chemistry
  ORGANIC CHEMISTRY LABORATORY:
  * 3 x 3 hours laboratories with associated write-ups.

  Learning Outcomes

  Students will become familiar with chemical descriptions of matter. What matter is made up of, how it can be organised into the periodic table and how we can start to understand it from a scientific perspective. They will learn about organic compounds and how they can be prepared, named and reacted.

  Skills

  Learners are expected to demonstrate the following on completion of the module:
  * Ability to write and predict atomic structure and properties.
  * Ability to explain and understand bonding.
  * Ability to recognise functional groups in organic chemistry and name compounds.
  * Ability to suggest reagents, mechanisms and reactions in organic chemistry.
  * Ability to demonstrate fundamental skills in laboratory practice and associated calculations.

  Coursework

  50%

  Examination

  0%

  Practical

  50%

  Credits

  20

  Module Code

  CHM1011

  Teaching Period

  Autumn

  Duration

  12 weeks

  Pre-requisite

  No

  Core/Optional

  Core

• Year 2

  Core Modules

  Safety and Mechanical Design (20 credits)

  ×

  Safety and Mechanical Design

  Overview

  Staff:
  Dr K Morgan 12 Lectures, 4 Tutorials: Mechanical Design Codes
  Dr D Poulidi
  d.poulidi@qub.ac.uk 15 Lectures, 4 workshops, 4 presentations: Process Safety Management
  Dr R Curry
  r.curry@qub.ac.uk 8 Lectures, 2 Tutorials / Seminars: Environmental Management
  
  
  Lectures: 48 hours
  1.Mechanical design codes (12 hours and 4 tutorials):
  * Standards, codes and codes of practice.
  * Design considerations.
  * Material selection of construction materials.
  * Mechanisms of failure.
  * Design of process equipment (Stress Analysis, Dimension sizing).
  * Design of auxiliary equipment.
  * Design of internal and external fixtures & fittings.
  * Critical Analysis Design.
  2.Process safety management – Accident and Loss (13 hours 2x2 hour presentations + 2x2hour workshops):
  * Overview and historical development of Process Safety Management.
  * Risk management: eliminating consequences, evaluating safeguards, assessing risk, implications of residual risk, control of land use, notifying neighbours and authorities, planning for emergencies, case studies; Hazard Identification (HAZID) studies, hazard and operability studies (HAZOP),
  * Mechanical integrity and Quality Assurance.
  * Τhe management of change.
  * Process safety. * Electrical and Fire Hazards and Control.
  * Chemical and Biological Health Hazards and Controls.
  * Physical and Psychological Health Hazards and Controls.
  * Accident Investigation, Recording and Reporting 3.Environmental Management (8 lectures + 2 tutorials hours)
  * Overview of the historical development of Environmental Management and recent developments such as Corporate Sustainability Appraisal.
  * Environmental Impact Assessment (EMA), guidance and approaches, identifying impacts and amelioration measures, recent developments in EMA and related policy and legislation.
  * Key metrics available for environmental management and wider sustainability appraisal including resource efficiency Sustainable Production and Consumption and Climate Change.
  * The Integrated Pollution Prevention and Control (IPPC) framework and recent developments.
  * Environmental Management Systems (EMS) and their relationship to wider management systems and corporate environmental policy.
  * The wider role of Chemical Engineers in Renewable Energy, Sustainable Production and Consumption and Climate Change. COURSEWORK: 150 hours:
  * Mechanical design of process equipment and ancillaries (55 hours): Process equipment used in the chemical industry often operates under severe conditions handling highly toxic, inflammable or hazardous substances. Students are required to take a pragmatic approach to the mechanical design of process equipment (e.g. absorption column/distillation tower) and auxiliary equipment (e.g. reboiler, condenser). Students will work in groups to complete a design problem related to the mechanical design of a piece of process/ancillary equipment. Students will be expected to research existing process equipment used in the chemical industry, material selection, complete analysis and evaluate design principles, complete design calculations (e.g. stress analysis, corrosion factors, geometry), critically evaluate their designs, apply BS EN 13445-3:2014 standards and select a suitable material to use in each problem. The final solutions will be reported in a written technical report of “professional standards” including calculations, references and graphical representation of designs using 2 or 3D CAD skills from CHE2018. This will prepare students for Mechanical Design in Level 3 Design II (CHE3014).
  * Accident case study report (55 hours): Students will be given a past industrial accident to investigate. Students will prepare a report including the following. A HAZID study of the process in question, a ‘what went wrong’ report including suggestions on measures that should have been taking in order to avoid the incident. A HAZOP study of the equipment responsible for the failure including the extra safeguards proposed by the students. This is a group project with individually marked elements.
  * Environmental Management (42 hours): Students are required to carry out an Environmental Impact Assessment for a sample company in the process industries and report on the key environmental metrics for company reporting. The students will work in groups for this.
  Note: Details on all coursework will be given out in the form of a coursework brief during term time. All coursework must be submitted electronically via QOL in the format specified in the coursework brief. Peer evaluation mark will contribute to 10% of the assignment mark unless differently stated in the coursework brief. Group reports may also include individual parts and part of the coursework may include other forms of assessment (e.g. presentations, class quiz); this will be detailed in the coursework brief.

  Learning Outcomes

  Learning outcomes:
  Students develop an awareness of the safe design, environmental impacts and operation of chemical process plants. By the end of this module students will be able to:
  • recognise the importance of safety and environmental management in chemical engineering design;
  • appreciate the impact of safety management incidents on the company, its employees, the wider public and the environment and of the ethical responsibility of engineers in preventing such incidents;
  • identify the various hazards associated with chemical processes;
  • discuss the range environmental impacts with chemical processes and more general plant operation;
  • apply the key aspects of Environment Impact Assessment;
  • employ key metrics available for environmental management;
  • relate the Environmental Management Systems (EMS) to wider management systems and corporate environmental policy;
  • apply the Integrated Pollution Prevention and Control (IPPC) framework in chemical plant design;
  • recognise the wider role of Chemical Engineers in Renewable Energy, Sustainable Production and Consumption and Climate Change;
  • use the relevant design codes, standards and legislation in chemical engineering design;
  • develop engineering judgement to support decision-making skills in ideas development and selection of appropriate materials and design calculations;
  • complete design calculations of chemical engineering equipment (stress analysis; equipment dimensions, pressure requirements)
  • critically evaluate the outcomes of mechanical design calculations and material selection;
  • understand mechanisms of failure, the mechanical design of process and auxiliary equipment;
  • select the appropriate materials for the design of process equipment;
  • appreciate the key aspects of Process Safety Management;
  • carry out a HAZOP study to identify and evaluate hazards in chemical processes;
  • carry out a risk assessment in a workplace environment

  Skills

  Skills acquired with module:
  An understanding of the use of design codes and the systematic use of process safety and environmental management and measurement procedures. The students will obtain the necessary theoretical background to carry out the mechanical design of process equipment and critically evaluate the safety and environmental hazards of a given chemical process. Via the range of required continual assessment the students will develop skills in report writing, group work and time management.

  Coursework

  100%

  Examination

  0%

  Practical

  0%

  Credits

  20

  Module Code

  CHE2106

  Teaching Period

  Full Year

  Duration

  24 weeks

  Pre-requisite

  No

  Core/Optional

  Core

  Process Control (20 credits)

  ×

  Process Control

  Overview

  STAFF
  
  NAME CONTRIBUTION
  
  Dr. M. Blesic m.blesic@qub.ac.uk
  Instrumentation and Computer Control Systems (14 hours);4 Tutorials.
  Mrs Evans LABS (2 hours)
  Dr. H. Manyar h.manyar@qub.ac.uk
  Module Co-Ordinator
  Process Control (35 hours); 8 Tutorials; 3 Seminars; Modelling of Chemical Processes (8 hours); 4 Tutorials.
  
  Process Control (25 hours):
  Incentives for process control in chemical plants.
  Design aspects of a process control system.
  Hardware for a process control system.
  Analysis of the dynamic behaviour of a chemical system.
  Process dynamics.
  Transfer functions.
  Response to first, second and higher order systems.
  Analysis and design of feedback control systems by frequency response-Bode plot.
  Block diagrams.
  Closed loop transfer functions.
  Stability.
  Rooth’s criterion.
  Root locus plot.
  Nyquist plot.
  Feedforward and ratio control.
  
  Modelling of Chemical Processes (8 hours):
  Introduction to process modelling.
  The development of a mathematical model.
  State Variables and State Equations for a Chemical Process.
  Dead-Time.
  Examples of Mathematical Modeling.
  Degrees of Freedom and process controllers.
  The dynamic and static behaviour of chemical processes.
  Laplace transforms.
  Solutions of ordinary differential equations.
  Partial fraction expansions (classical and Heaviside’s methods).
  
  Instrumentation and Computer Control Systems (14 hours):
  Basic principles of measurement and control.
  Control system instrumentation.
  Signal processing.
  Accuracy in instrumentation.
  Single-loop regulatory control.
  On-off controllers.
  Proportional control.
  Integral control.
  Derivative control.
  PID control.
  Enhanced control strategies.
  Feed-forward control.
  Cascade control.
  Ratio control.
  Split-range control.
  Override control.
  Interlock control.
  Piping and Instrumentation Diagrams.
  Control strategies at the process unit level.
  Batch process control.
  Batch control systems.
  Sequential function charts.
  Ladder logic diagrams.
  Applications.
  S88.01 standard.
  Recipe control.
  Procedural control.
  Coordination control.
  Digital computer control.
  Direct digital control systems.
  Programmable logic controllers.
  Distributed control systems.
  Process control in biochemical reactors.
  Methods of instrumental analysis.
  
  Tutorials/Seminars (17 Hours):
  The students are provided with tutorial, worked examples, seminar, SIMULINK assignments and laboratory experiments related to the above lecture material. Tutorials will take place both in class and in small groups. During the tutorials, the students will work through the problems with focus on design of control strategies, instrumentation, stability analysis and computational methods for development of plant wide process control while seminar will include a tour to combined heat and power (CHP) plant, an assignment concerning process control, safety and risk assessment of CHP plant.
  
  LABS (2 hours):
  Students will be divided into groups. Each group will carry out following experiment:
   1.Temperature Control in a Process Vessel (2 hours)
   Both an individual pre-lab report and an individual post-lab report will be submitted for each experiment as indicated in the lab manual (to be handed out in the beginning of the term

  Learning Outcomes

  Upon completion of the module the student should be familiar with developing an awareness of the control and instrumentation required in chemical process operations, should be competent in setting fundamental procedures for process units and should gain skills to develop the control strategy and instrumentation required in the process plant operations. By the end of the module the students should:
  
  • Identify and describe various control systems
  • Describe various hardware of process control design;
  • Analyse the dynamic behaviour of a chemical system;
  • Predict and calculate the response to first, second order and higher order systems;
  • Design feedback, feedforward and ratio-control systems by using stability criteria of Bode, Nyquist and root locus plots;
  • Construct and analyse control loops using Simulink;
  • Produce piping and instrumentation diagrams;
  • Apply various control systems: discrete control; batch control; digital computer control and distributed control systems.

  Skills

  Skills acquired with module:
  An appreciation of the fundamental principles of process control and instrumentation in chemical engineering design.

  Coursework

  30%

  Examination

  70%

  Practical

  0%

  Credits

  20

  Module Code

  CHE2103

  Teaching Period

  Full Year

  Duration

  24 weeks

  Pre-requisite

  No

  Core/Optional

  Core

  Chemical Plant Design and Operation (20 credits)

  ×

  Chemical Plant Design and Operation

  Overview

  Dr. J. Abu-Dahrieh j.abudahrieh@qub.ac.uk
  2. Computer Lab Classes; Section 1. Review and Analysis of Production Process
  Dr. M. Blesic - m.blesic@qub.ac.uk
  Section 3. Chemical Design; Section 4. Process Control and Operation
  Dr. N. Gui Email: m.gui@qub.ac.uk
  Section 2. Heat and Mass Balances
  Dr. C. Mangwandi
  c.mangwandi@qub.ac.uk
  1. Mathematics and numerical methods; 2. Computer Lab Classes and assessment;
  Dr. E. Themistou –e.themistou@qub.ac.uk 3. Process Economics
  Dr. Chunfei Wu c.wu@qub.ac.uk
  2. Computer Lab Classes and assessment; Section 2. Heat and Mass Balances
  
  Course content
  1. Mathematics and numerical methods (6 hours, 3 tutorials):
   Revision of ordinary differential equations (ODEs) and initial value problems. Application to first order reactions. Solution by quadrature;
   System of first order ODEs and initial value problems. Application to chemical kinetics. Solution by Laplace transform and associated linear system. Revision of Cramer's rule. Gaussian elimination;
   Reduction of a higher order ODE to a system of first order ODEs. Nonlinear ODEs and numerical solution by the Euler method. Local and global error. Runge-Kutta methods. Application to chemical kinetics;
   Matlab revision Class.
  
  2. Computer Lab Classes and assessment:
   Students are provided with online tutorials. Students will also have the opportunity to be offered summary computer lab class in each of the core areas.
  
   Aspen
   AutoCAD (self-learning)
   Excel
   Matlab
   Class tests on Aspen and Matlab
  
  3.Process Economics (9 hours)
   Basics of process economics including financial statements, depreciation, interest, IRR, NPV
   
  4. Chemical Plant Design
  Section 1. Review & Analysis of Production Method (6 hours):
   Review and analyse the production process.
   Source and use key physical property data for design purposes.
   Provide detail process description and refine the PFD of the production process.
   Produce an initial report including a preliminary mass balance.
  
  Section 2. Heat and Mass Balances (16 hours):
   Conduct detailed heat and mass balances on all unit operations in the plant including use of Excel models.
   Develop an Aspen simulation model of the process.
   Report the heat and mass balances.
  
  Section 3. Chemical Design (10 hours):
   Provide a detailed chemical engineering design for a main unit (multistage gas compressor, heat exchanger, distillation column):
   Equipment type.
   Major vessel dimensions (size, shape).
   Internals (trays, packing, agitator, baffles, etc.).
   Using AutoCAD, generate a drawing detailing the results obtained from above considerations.
  
  Section 4.Process Control and Operation (6 hours)
   Develop and report a control strategy for a specific unit.
   Identify and report operational and health & safety issues.
   Using AutoCAD generate a drawing detailing the control system
   Prepare start-up and shut-down procedures for a specific unit.
   Prepare a complete HAZOP report for a specific unit.

  Learning Outcomes

  Students will obtain a foundation in chemical engineering design using a given process example. By the end of the course, the students will be able to:
  
  • effectively use computer software including Excel, Matlab, Aspen and AutoCad as tools for solving chemical engineering design problems and presenting flow-sheets and equipment
  • identify appropriate mathematical equations and tools needed to support other core modules at stage 2 and beyond
  • apply numerical methods for solving complex engineering design problems
  • source and evaluate key physical property data from the literature, or computer databanks for design calculations
  • use a computational language (e.g., Matlab) for the development of computer code needed to solve chemical engineering problems
  • apply the overall heat and mass balances and conceptual process flow diagrams (PFD) in solving chemical engineering problems.
  • explore design and operational considerations for a chemical plant
  • produce a suitable plant layout
  • develop appropriate health, safety and environmental guidelines
  • produce a final design report
  • develop and apply knowledge of financial costing and accounting systems to evaluate process economics.

  Skills

  Students will develop skill in the use of specific computer software to solve chemical engineering problems and sketch flow-sheets or equipment Moreover, the module will develop skills in plant operation and in the design and development of a chemical engineering production process including skills in identifying and articulating environmental impacts and operational protocols. Specific skills include:
  
  • improved mathematical and problem solving skills
  • computational skills will be developed through use of specific and general computer packages for solving chemical engineering design problems
  • P&ID reading
  • literature reviews and data selection
  • analytical and computational
  • communication and reporting
  • team and individual working
  • time management
  • costing and financial analysis skills.

  Coursework

  100%

  Examination

  0%

  Practical

  0%

  Credits

  20

  Module Code

  CHE2105

  Teaching Period

  Full Year

  Duration

  24 weeks

  Pre-requisite

  No

  Core/Optional

  Core

  Heat and Mass Transfer (20 credits)

  ×

  Heat and Mass Transfer

  Overview

  NAME CONTRIBUTION
  Dr. M. Blesic Module Co-ordinator
  m.blesic@qub.ac.uk Forced Convection (5 hours) ; Natural Convection (3 hours); Heat Exchangers (6 hours): Unsteady State Heat Transfer (6 hours); Tutorials: Forced and natural convection (2 hours);
  Heat exchangers (3 hours);Unsteady state heat transfer (2 hours);
  Mrs S. Evans - Email: s.evans@qub.ac.uk Labs (9 hours)
  Dr. N. Gui,
  M.Gui@qub.ac.uk Distillation (9 hours); Solvent Extraction (4 hours); Interphase and General Mass Transfer (3 hours); Gas Absorption (5 hours); Tutorials: 5.Distillation (3 hour);Solvent extraction (3 hour)
  ;Interface and general mass transfer (2 hour);Gas absorption (2 hour);
  Dr E. Themistou
  e.themistou@qub.ac.uk Radiative Heat Transfer (5 hours); Radiative heat transfer (2 hours);
  
  Detailed Syllabus - Lectures:
  Radiative Heat Transfer (5 hours):
   Modes of Heat Transfer.
   Emission and absorption of radiation.
   Definitions and laws of radiation.
   Photon gas
   Blackbody and real surface radiation.
   Effects of incident radiation - absorptivity, reflectivity and transmissivity.
   Radiative shape factors for simple and complex geometries.
   Radiation between surfaces – relations between radiative shape factors.
   Surface energy balance for opaque material – irradiation and radiosity.
   Radiation between non-black surfaces, electrical analogies.
   Insulated surfaces, surfaces with large areas infinite parallel surfaces
  
  Forced Convection (5 hours):
   Physical mechanism of forced convection.
   Newton's Law of cooling.
   Convective heat transfer coefficient.
   Nusselt number.
   Velocity boundary layer.
   Boundary layer theory and friction and drag coefficients.
   Laminar and turbulent flows.
   The Reynold number.
   Thermal boundary layer.
   Thermal boundary layer theory.
   Prandtl number.
   Flow over flat plates.
   Flow across cylinders and spheres.
   Flow in tubes.
   Constant heat flux.
   Constant surface temperature.
   Logarithmic mean temperature difference.
   Pressure drop.
   Flow regimes in a tube.
   Hydrodynamic and thermal entry lengths.
   Laminar flow in tubes.
   Turbulent flow in tubes.
  
  Natural Convection (3 hours):
   Physical mechanism of natural convection, volume expansion coefficient, Grashof number.
   Natural convection over surfaces, natural convection correlations, natural convection inside enclosures.
   Combined natural and forced convection.
  
  Heat Exchangers (6 hours):
   Heat exchange.
   Applications and types of heat exchangers.
   Selection of heat exchangers.
   Temperature profile in heat exchangers.
   Basic equations in heat exchanger design.
   Overall heat transfer coefficient.
   Fouling factors.
   Log mean temperature difference (LMTD) – calculation for parallel-flow and counter-flow heat exchangers.
   LMTD - special operating conditions for condensers, evaporators/boilers.
   LMTD correction factors for multipass and cross-flow shell-and-tube heat exchangers.
   The heat exchanger effectiveness (ε) – number of transfer units (NTU) method for heat exchanger analysis for various types of heat exchangers.
   Shell-and-tube heat exchanger design.
   Design procedure, construction details and design considerations.
   Tube-side and shell-side heat transfer and pressure drop.
   Design methods: Kern’s and Bell methods.
   Gasketed-plate heat exchanger applications and design: Heat transfer area, mean flow channel gap, channel hydraulic diameter, heat transfer coefficient, total pressure drop, overall heat transfer coefficient, heat transfer surface area, thermal performance.
   Condensation and boiling.
  
  Unsteady State Heat Transfer (6 hours):
   Introduction.
   Unsteady state conduction equation.
   Lumped capacitance method.
   Unsteady state heat conduction in various geometries: analytical method, semi-infinite solid, unsteady state in large flat plates.
   Charts for average temperature in plates, cylinders and spheres with negligible resistance.
   Numerical methods for unsteady state: finite difference, boundary conditions, selected applications.
   Boundary layer flow and turbulent conditions.
   0D to 3D transient problems.
  
  Distillation (9 hours):
   Vapour pressure introduction: Vapour-liquid equilibria, Raoult’s law, Henry’s law, Dalton’s law, steam distillation, relative volatility, azeotropic systems.
   Flash distillation – material and energy balance equations, operating lines.
   Flash cascades.
   Isothermal flash configuration – multicomponent:
   Rachford-Rice equations.
   Newton’s iterative method for solving Rachford-Rice equations.
   Plate columns.
   McCabe-Thiele method for special equipment:
   Total and partial condenser.
   Sub-cooled reflux.
   Total and partial reboiler.
   Live steam injection.
   Multiple feeds.
   Side streams.
   Ponchon Savarit method for binary distillation.
   Enthalpy-composition diagrams.
   Equilibrium-stage calculations.
  
  Solvent Extraction (4 hours):
   Liquid-liquid extraction introduction.
   Examples of ternary systems and ternary phase diagrams.
   Review of processes and applications.
   Review of equipment.
   Totally and partially immiscible systems.
   Stagewise contact:
   Single-stage extraction.
   Multistage crosscurrent extraction.
   Continuous countercurrent multistage extraction.
   Cascade efficiencies.
  
  Interphase and General Mass Transfer (3 hours):
   General introduction to turbulent mass transfer.
   Film theory and surface renewal.
   Two-film theory.
   Individual and overall mass transfer coefficients.
   Steady state co-current and counter-current processes (operating and equilibrium lines).
   Mass transfer with continuous contact: height equivalent to a theoretical plate, the transfer unit, determination of the number of transfer units, determination of the number of transfer units, height of a transfer unit.
   Mass transfer with discontinuous contact.
  
  Gas Absorption (5 hours):
   Gas-liquid equilibria.
   Choice of solvent for absorption.
   Counter-current and co-current flow.
   Minimum liquid-gas ratio for absorbers.
   Number of plates using absorption factor.
   Absorption columns.
  
  Detailed Syllabus –Tutorials (19 Hours):
  The students are provided with tutorial and worked examples of the above lecture material. Tutorial classes are an integral element of the module.
  
   1.Radiative heat transfer (2 hours) – Dr E. Themistou
   2.Forced and natural convection (2 hours ) - Dr. M. Blesic
   3.Heat exchangers (3 hours) – Dr. M. Blesic
   4.Unsteady state heat transfer (2 hours ) - Dr. M. Blesic
   5.Distillation (3 hour) - Dr. N. Gui
   6.Solvent extraction (3 hour) - Dr. N. Gui
   7.Interface and general mass transfer (2 hour) - Dr. N. Gui.
   8.Gas absorption (2 hour) - Dr. N. Gui.
  
  Detailed Syllabus – Labs (9 Hours):
   Students will be divided into groups. Each group will carry out experiments based on:
  
   1. Boiler Heat Transfer Unit (2 hours)
   2. Turbulent Flow Counter-Current Heat Exchanger (2 hours)
   3. Distillation column (2 hours)
   4. Liquid/liquid extraction (2 hours)
   5. Gas absorption column (1 hour)
  
   Both an individual pre-lab report and an individual post-lab report will be submitted for each experiment as indicated in the lab manual (to be handed out at the beginning of the term).

  Learning Outcomes

  On completion of this module a learner should be able to:
   General Learning Outcomes:
   Develops an understanding of how heat transfer is accomplished in chemical engineering process operations and applies the concept of mass transfer to specific unit operations such as distillation and solvent extraction.
   Specific Learning Outcomes:
   On completion of this module the student should:
   Understand the concept of heat, interphase and mass transfer;
   Be able to calculate heat transfer rates using correlations of non dimensional groups, analytical techniques or numerical techniques;
   Understand the compromises between effectiveness and cost inherent in the design optimisation of heat transfer equipment;
   Understand in depth the unsteady state heat transfer which is essential in start-up and transient processes;
   Acquire basic knowledge of radiation heat transfer which is essential for the design of higher temperature systems.
   Develop and apply the concept of mass transfer to specific unit operations including distillation, solvent extraction, absorption and adsorption.
   Recognise, analyse, compare and choose from various cases of distillation design such as flash distillation, multiple feeds, side streams and live steam injection.
   Design azeotropic distillation processes.
   Apply the concept of mass transfer in extraction processes.
   Design crosscurrent and countercurrent multistage extraction processes.
   Use the concept of interphase and general mass transfer.
   Solve problems on mass transfer with continuous contact.
   Explain the concepts of mass transfer in gas absorption and adsorption processes.
   Design methods for gas absorber analysis.
   be able to apply mass transfer in leaching processes;
   Design of cocurrent and countercurrent leaching processes.
   Improved understanding of basic chemical engineering (heat transfer, vapour pressure, bubble points, distillation, heat exchange etc.) through specific test questions.
   Obtain a greater understanding of overall heat and mass balances and conceptual process flow (PF) diagrams.

  Skills

  Learners are expected to demonstrate the following on completion of the module:
   Application of the concepts of heat transfer and design to heat transfer systems.
   An appreciation of the design and operation of mass transfer process.
   Improved mathematical and problem solving skills.
   An ability to use specific and general computer packages for solving chemical engineering design problems.
   Ability to utilise specific chemical engineering application software in solving chemical engineering problems, such as Matlab.

  Coursework

  30%

  Examination

  50%

  Practical

  20%

  Credits

  20

  Module Code

  CHE2102

  Teaching Period

  Full Year

  Duration

  24 weeks

  Pre-requisite

  No

  Core/Optional

  Core

  Fluid Mechanics (20 credits)

  ×

  Fluid Mechanics

  Overview

  STAFF
  
  NAME CONTRIBUTION
  Dr. M. Blesic
  m.blesic@qub.ac.uk Fluid Mechanics (10); Mixing of liquids (3); Filtration and centrifugation (3); Heat and Mass Transfer in Fluidised Systems (5); Tutorials;
  Dr. C. Mangwandi
  c.mangwandi@qub.ac.uk Module Co-Ordinator
  Particle mechanics (10); Size reduction, separation & classification (10);Non- Newtonian Fluids (10); Tutorials;
  Dr. B. Xiao
  b.xiao@qub.ac.uk
  Transport Phenomena (9); Tutorials.
  Content
  
  Fluid Mechanics (10):
   Fundamentals.
   Transport Laws.
   Dimension Analysis.
   Scale-up.
   Dimensionless Groups in Fluid Mechanics.
   Fluid Properties.
   Fluid Kinematics.
   Finite Control Volume Analysis.
   Differential Analysis of Fluid Flow, Flow in Pipes.
   Pumps and Compressors.
   Flow Over Immersed Objects.
  
  Mixing of liquids (3):
   Introduction.
   Liquid-liquid mixing equipment.
   Installation of mixers and tank baffling.
   Power consumption and mixing theory.
   Impellor and process power selection.
  
  Particle mechanics (10):
   Characteristics of particles, rheology of particle masses and gravity flow of bulk solids.
   Pressure drop through beds of particulate solids.
   Drag.
   Potential flow and flow of a real fluid.
   Flow separation and wake formation.
   Drag coefficients, drag diagrams and relationships.
   Terminal velocity in an infinite medium and hindered settling.
   Accelerated motion in free settling.
   Fluidisation:
   Types of fluidisation systems
   Minimum fluidisation velocities
  
  Filtration and centrifugation (3):
   Gas and liquid filtration equipment.
   Kozeny equation.
   Constant pressure filtration.
   Constant rate filtration.
   Incompressible and compressible cakes.
   Depth and cake filtration in gas-solid systems.
   Centrifugation
   Centrifugal equipment.
   Centrifugal force and fluid pressure.
   Liquid-liquid separation.
   Solid-liquid filtration using centrifuge.
   Wall stresses.
  
  
  
  Size reduction, separation & classification (10):
   Size reduction, Von Rittinger's, Kick's laws and Bond's laws, work index, energy size reduction and size reduction equipment.
   Size classification, equipment, Stoke's law, free and hindered settling:
   Gas – Solid separation:
   Cyclones
  
  Transport Phenomena (9):
   Shell Momentum Balances:
   Boundary Conditions
   Velocity Distributions in Laminar Flow
   Flow of a Falling Film
   Flow Through a Circular Tube
   Through an Annulus
   The Equations of Continuity and Equations of Motion
   Velocity Distributions with More Than One Independent Variable
   Time Dependent Flow of Newtonian Fluids:
   Flow Near Solid Surfaces by Boundary Layer Theory
   Thermal Conductivity and the Mechanisms of Energy Transport
   Shell Energy Balances
   Boundary Conditions
   Temperature Distributions in Solid and Laminar Flow
   Diffusivity and the Mechanisms of Mass Transport
   Concentration Distributions in Solids and Laminar Flow
  
  Non- Newtonian Fluids (10):
   Introduction to rheology
   Models for non-Newtonian Fluids:
   Power law fluids
   Bingham model
   Ellis Model;
   Carson Model.
   Incompressible Flow of Non-Newtonian Fluid in simple geometries:
   Power Law
   Bingham
   Slurry transport
   Measurement of Viscosity
   Capillary Viscometers
   Cone & Plate viscometers
  
  Heat and Mass Transfer in Fluidised Systems (5):
   Bubbling Fluidisation System
   Modelling of Gas Flow in Fluidised System
   Heat Transfer in Gas Flow Fluidised System
   Examples of Industrial Application of Fluidised Systems
   Batch Fluidised Systems
   Continuous Fluidised Systems
   Modified Gas-Liquid Fluidisation Systems
   Babble Droplet Dispersion
  
  Tutorials/seminars:
  The students are provided with tutorial, worked examples of the above lecture material. Tutorials/seminars are an integral element of the module.

  Learning Outcomes

  On completion of this module a learner should be able to:
   Demonstrate an understanding of behaviour and characteristics of fluids in process unit operations, and theory and application of transport phenomena.
   By the end of the module the students will have:
   have developed an understanding of the fluid flow, Naiver Stokes equations; be able to apply these equations when solving fluid flow problems;
   have the ability to correctly design fluid delivery systems, sizing of pumps and pipe to ensure economic transportation of fluids;
   developed methodologies for designing and sizing and scaling up of fluids mixing operations; awareness of the use of different scale up rules and when they are appropriate to apply these;
   developed an awareness of industrial/practical hydrodynamic efficiency in terms of pressure drop in pipeline and fixed bed systems, and drag coefficients for solid bodies;
   be able to select correct tools required for designing and sizing the size reduction unit operations
   developed methodologies for selecting and design appropriate unit operations of separation/ recovery of solids from solid/ fluid stream mixtures;
   developed an appreciation of size enlargement unit operations, able to identify and describe the key variables that influence the product quality;

  Skills

  SKILLS ACQUIRED:
  • Numerical skills through application of transport phenomena in process engineering,
  • Analytical – Evaluation of data and its use in design.
  • Problem solving skills

  Coursework

  20%

  Examination

  60%

  Practical

  20%

  Credits

  20

  Module Code

  CHE2104

  Teaching Period

  Full Year

  Duration

  24 weeks

  Pre-requisite

  No

  Core/Optional

  Core

  Chemical Process Thermodynamics (20 credits)

  ×

  Chemical Process Thermodynamics

  Overview

  STAFF
  
  NAME CONTRIBUTION
  Dr J. Abu-Dahrieh
  j.abudahrieh@qub.ac.uk
  10 Lectures, 3 Tutorial/Seminars: Design of Ideal reactors,10 Lectures and 3 tutorials/seminars; Design of ideal reactors (2 hours – 1 assessed tutorial); Chemical Thermodynamics (4 hours - 1 assessed tutorials);
  Mrs S. Evans Labs (6 Hours).
  Prof A. Mills
  andrew.mills@qub.ac.uk
  8 Lectures, 1 Tutorial/Seminar: Basic reaction kinetics,8 Lectures and 1 tutorial; Basic reactor kinetics (1 assessed tutorial);
  Dr Kevin Morgan
  k.morgan@qub.ac.uk
  14 Lectures, 6 Tutorial / Seminars:Chemical Thermodynamics,14 Lectures and 6 tutorials/seminars;
  Dr D. Poulidi Module Co-ordinator
  d.poulidi@qub.ac.uk
  14 Lectures, 6 Tutorials/Seminar: Consequences and applications, 14 Lectures and 6 tutorials; Chemical Engineering Thermodynamics (2 hours - 1 assessed tutorial).
  
  
  Detailed Syllabus – Lectures: Basic reaction kinetics (8 Lectures and 1 tutorial):
  * 1.1 Introduction to reaction kinetics.
  * 1.2 rate law and reaction order.
  * 1.3 reaction stoichiometry.
  * 1.4 molecularity, elementary and non-elementary reactions.
  * 1.5 order of reaction.
  * 1.7 single and multiple reactions, parallel and series reactions, multi-step processes,
  * 1.8 Arrhenius equation, manipulation and use of rate equations.
  * 1.9 interpretation of experimental kinetic data. * 1.10 integrated rate equations, equilibria kinetics.
  Design of Ideal reactors (10 Lectures and 3 tutorials/seminars):
  * 2.1. Development of design equations for batch and continuous reactors. * 2.2. Conversion and reactor sizing.
  * 2.3 Reactors in series and in parallel.
  * 2.4. Construction of stoichiometric tables.
  * 2.5 Application of chemical kinetic rate equations in the design of isothermal reactors.
  * 2.6 Review of chemical equilibrium, application of chemical equilibrium in reactor design.
  * 2.7 Reactors in series and in parallel, optimization of reactors.
  * 2.8 Multiple reactions.
  * 2.9 Temperature and pressure effects.
  * 2.10; Introduction to non-ideal reactors.
  Chemical Thermodynamics (14 Lectures and 1 tutorials/seminars):
  * 3.1 Introduction.
  * 3.2 PVT properties of fluids - equations of state: ideal and non-ideal gases, critical properties, reduced properties and principle of corresponding state, generalised equations of state, analytical equations of state.
  * 3.3 Review of the first, second and third laws of thermodynamics.
  * 3.4 Relationships among thermodynamic properties: basic relations, Maxwell relationships, Bridgeman tables.
  * 3.5 Fugacity and fugacity coefficients: partial molar properties, chemical potential, the concept of fugacity, estimating the fugacity of a pure component.
  * 3.6 Multicomponent systems: liquid and solid fugacity, Gibbs-Duhem equation, partial fugacity, ideal mixtures, non-ideal mixtures, standard states.
  * 3.7 Physical equilibrium among phases: the phase rule, criteria for phase equilibrium, vapour-liquid equilibrium, equilibrium phase diagrams. Chemical Engineering Thermodynamics: concepts, consequences and applications (14 Lectures and 3 tutorials / seminars):
  * 4.1 Review of thermodynamic diagrams and water and steam properties; * 4.2 Power from steam: plant efficiency, power plant cycle analysis, superheat, reheat and regenerative feed heating, future performance improvements;
  * 4.3 Types of refrigeration, review of important gas laws, thermodynamic principles and vapour compression cycles (Refrigeration cycles, COP, Cooling load calculations;
  * 4.4 Tools to solve non-ideal Chemical Engineering Thermodynamics problems (Equation of State and activity-coefficient models)
  
  Detailed Syllabus – Seminars/Marked Tutorials/ Class Tests:
  * Seminars / problem classes will be part of the module content. The hours allocated for these are part of the tutorial / seminar allocation shown above.
  * Two class tests, each contributing 15% of the final module mark will take place. Details on the dates and content of the class tests will be communicated to students in the beginning of the semester. Detailed Syllabus – Labs (6 Hours):
  * Students will be divided into groups. Each group will carry out experiments based on: * Batch Reactor (2 hours);
  * Refrigeration Unit (2 hours).
  * Both an individual pre-lab report and an individual post-lab report will be submitted for each experiment as indicated in the lab manual (to be handed out at the beginning of the term).

  Learning Outcomes

  On completion of this module a learner should be able to:
  Define different types of reactors.
  Describe the role of reactors within modern chemical processes.
  Apply knowledge of equilibrium, molecularity, mole balances, etc.to kinetic and reaction engineering problems.
  Develop basic principles of kinetics and reactor design.
  Use basic kinetic and thermodynamic knowledge for the design of ideal reactors found in industry.
  Understand the concepts of reactors in series and parallel.
  Use mathematics for solving reactor design problems;
  Calculate the implications of selectivity and yield on downstream processing.
  Design different types of ideal reactors.
  Understand and apply equation of state models to relevant thermodynamic problems.
  Evaluate thermodynamic cycles for power generation and cooling.
  Apply knowledge of industrial/practical thermal efficiency to improving energy consumption

  Skills

  Design of simple reactor systems; Mathematical and analytical skills through application of thermodynamic equations in reactor design.
  Module Objectives: Students will be able to understand and apply the basic concepts of chemical reactor design and chemical thermodynamics to chemical engineering problems. Students will be able to evaluate the influence of thermodynamics on process operations and design.

  Coursework

  30%

  Examination

  60%

  Practical

  10%

  Credits

  20

  Module Code

  CHE2101

  Teaching Period

  Full Year

  Duration

  24 weeks

  Pre-requisite

  No

  Core/Optional

  Core

• Year 3

  Core Modules

  Biochemical Engineering (10 credits)

  ×

  Biochemical Engineering

  Overview

  module co-ordinator
  Dr Efrosyni Themistou
  e.themistou@qub.ac.uk
  LG.440 David Keir Building
  
  Detailed Syllabus – Lectures (28 hours):
  
  Introduction to Biochemical Engineering (2 hours):
   Overview on Biomedical and Biotechnology Industries.
   Cells/microorganisms.
  
  Enzyme Kinetics (4 hours):
   Enzymes Introduction: Biological catalysts and systems, comparison of chemical processes and bioprocesses.
   Kinetics of enzyme catalysed reactions - mechanistic models: Michaelis-Menten kinetics for reversible reactions, two-substrate reactions and enzyme inhibition.
   Factors affecting enzyme activity.
  
  Cell Kinetics, Bioreactor Design and Sterilisation (8 hours):
   Kinetics of cell growth, substrate utilisation and product formation - Monod kinetics.
   Batch and continuous stirred tank bioreactors.
   Environmental effects on cell growth kinetics.
   Microorganism growth - biology, profile, processing and products.
   Sterilisation: kinetics of thermal deactivation, design of heat sterilization cycles.
  
  Industrial Microbiology (9 hours):
   Fermentation Systems (Beverage and Food).
   Environmental Biotechnology.
   Aerobic and anaerobic digestion.
  
  Biomaterials (5 hours):
   Introduction to Biomaterials and their applications.
   Biomaterials processing, structure and properties.
   Classes of Biomaterials (Polymers, Metals and Ceramics).
  
  Detailed Syllabus – Tutorials/Seminars (5 hours):
  The students are provided with tutorials - worked examples related to the above lecture material. Seminars will focus on methodologies for creative problem solving and reading.
  
   Enzyme Kinetics (2h)
   Cell Kinetics (1h)
   Biomaterials (1h)
   Seminar (revision) (1h)
  
  Detailed Syllabus – Coursework/Class Tests (2 staff hours):
  Class Tests (2h)

  Learning Outcomes

  On completion of this module students should be able to:
   Acquire a knowledge of biomaterials and biomedical engineering, system and device design, their applications in healthcare and related ethical issues (coursework and exam).
   Develop an understanding of the interface between life science, biology, advanced mathematics, biological and biomedical systems in the context of engineering (exam).
   Demonstrate a knowledge of industrial microbiology (exam).
   Formulate and solve interdisciplinary problems in engineering and biology using growth models, cell and enzyme kinetics (exam).
   Apply their knowledge in chemical engineering to design systems for living organisms, such as batch and continuous bioreactors (exam).
  
  Engineering Council (AHEP4) learning outcomes:
  A1.2 Level B Points 3,4,5 and Level F Point 1
  A2.2 Level B Point 5
  A2.4 Level B Point 1
  A2.5 Level B Point 1 and Level F Point 1
  A2.6 Level B Point 1
  A2.7 Level B Points 1,3,5 and Level F Point 1
  A3.2 Level B Points 2,4,9,10,11 and Level F Points 1,2,3,4
  A5.2 Level B Points 1,2 and Level F Points 2,4,5,8
  A6.2 Points 2,3

  Skills

  Learners are expected to demonstrate the following on completion of the module:
   An understanding of biomaterials, biomedical engineering and industry, enzyme and cell kinetics; microorganisms, bioreactor and bioprocess design; industrial microbiology.
   Gained transferrable skills:
   Independent learning through background reading of scientific literature, time management and problem-solving (exams, tutorials, and seminars).

  Coursework

  30%

  Examination

  70%

  Practical

  0%

  Credits

  10

  Module Code

  CHE3008

  Teaching Period

  Spring

  Duration

  12 weeks

  Pre-requisite

  No

  Core/Optional

  Core

  Chemical Reactor Design and Process Integration (30 credits)

  ×

  Chemical Reactor Design and Process Integration

  Overview

  Staff:
  NAME CONTRIBUTION
  Jehad Abu-Dahrieh Thermodynamics of Chemical Reactions
  Kevin Morgan Catalysts and catalytic reactors.
  Alex Goguet (Module Co-ordinator) Reactor Theory And Design
  John Holbrey Resources in the Energy and Chemical Industries
  Alex Goguet Optimisation of catalytic reactions
  Danai Poulidi Exergy analysis and Process Integration
  Abul Hassan Reactor Design and Simulation Techniques
  Abul Hassan Multiphysics CFD Simulation for Reactor Design
  
  Semester 1:
  
  Reactor Theory And Design (14/10) Alex Goguet:
  Revision of chemical kinetic fundamentals; revisions of basic design methods; description of different types of chemical reactors.
  Reversible reactions; irreversible reactions; single, parallel, and consecutive reactions; constant volume systems; the concept of fractional conversion; variable volume reactions and reactor systems; plug flow reactors; and continuous stirred tank reactors.
  Heat effects in chemical reactor design; the temperature dependence of rate constant; exothermic reactions; endothermic reactions; heat effects in irreversible and reversible reactions; the relationship between heat of reaction and temperature rise/fall; adiabatic heat balances in continuous flow reactors; the optimum temperature profile; the design of adiabatic reactors for endothermic, exothermic, irreversible and reversible reactions.
  Flow effects in reactors; the concept of dead space, short circuit flow and bypassing in stirred vessels; the concept of dead space, laminar flow, channelling and axial mixing in tubular flow reactors; the concept of residence time distribution in continuous flow reactors; the determination of residence time data; tracer response techniques; the E function; the F function; the application of residence time distribution data in reactor design; introduction to modelling of non-ideal flow in continuous flow reactors; the stirred tanks in series model; the dispersion model.
  
  Catalysts And Catalytic Reactors (16/8) Kevin Morgan:
  Rate equation for heterogeneous reactions.
  Rate controlling mechanisms.
  Experimental methods for rate determination.
  Decomposition of a single reactant by two paths.
  Side-by-side decomposition by two reactants.
  Adiabatic operations.
  Components of typical heterogeneous catalysts.
  Industrial preparation of supported catalysts.
  
  Reactor Design and Simulation Techniques (6/10) Abul Hassan:
  Introduction to reactor process flowsheeting and simulation with Aspen Suite
  Thermodynamic principles and catalyst performance using Aspen
  Continuous Stirred Tank Reactor (CSTR)
  Plug Flow Reactor (PFR)
  Conversion Reactor
  Equilibrium Reactor
  Gibbs Reactor
  Troubleshooting simulation challenges
  Exploring open-source alternatives with COCO Simulator
  
  Semester 2:
  
  Optimisation Of Catalytic Reactions (8/4) Alex Goguet:
  Catalyst deactivation and design for catalyst deactivation.
  Effect of pressure drop.
  Reactor optimisation.
  
  Thermodynamics of Chemical Reactions (8/3) Lecturer Jehad Abu-Dahrieh:
  Revision of physical properties of pure component and mixture.
  Multicomponent mixtures.
  Chemical reaction equilibrium.
  Multireaction equilibria.
  Prediction of thermodynamics properties and phase behaviour using equation of state.
  Modelling of thermodynamic systems.
  
  Exergy analysis and Process Integration (12/4) Danai Poulidi:
  Exergy and Pinch Technology.
  Minimum targets.
  Design rules.
  Energy relaxation.
  Grand composite curves.
  Utility design.
  Retrofit design.
  
  Resources in the Energy and Chemical Industries (6/1 workshop) John Holbrey:
  Changes taking place in the energy and chemicals industries as we move from petrochemical to renewable resources,
  Using case studies to illustrate the drivers and technologies available to supply current and future energy and materials demands.
  
  Multiphysics CFD Simulation for Reactor Design (2/6) Abul Hassan:
  Introduction to COMSOL Multiphysics
  Basic Reactor Model Setup in COMSOL
  Simulating Basic Chemical Reactions in COMSOL
  Introduction to Open-Source CFD with OpenFOAM

  Learning Outcomes

  LO1 Review and apply the basic principles of kinetics and reactor design to the design of ideal reactors found in industry.
  LO2 Be aware of the concepts of selectivity and yield and the downstream implications of adjusting reactor operating conditions
  LO3 Understand the importance of thermal control of chemical reactions and the implications of poor control with regard to process safety.
  LO4 Be aware of the impact of non-ideal flow on product yields.
  LO5 Understand the importance of catalysis to modern industry and have an increased knowledge relating to the application of catalysts in industry, their manufacture and operation within reactors.
  LO6 Demonstrate knowledge relating to the impact of mass transfer on multi-phase chemically reacting systems.
  LO7 Understand the principles of momentum, heat and mass transfer and application to problems involving fluids and multiple phases.
  LO8 Be aware of the complexities of integrating, pressure drop, non-isothermal, catalyst deactivation etc. when solving more complex chemical engineering design problems.
  LO9 Demonstrate knowledge of the principles of equilibrium and chemical thermodynamics, and application to phase behaviour, to systems with chemical reaction and to processes with heat and work transfer.
  LO10 Analyse more complex thermodynamic cycles under the principles of equilibrium and chemical thermodynamics.
  LO11 Understand the concepts of process integration and exergy analysis.
  LO12 Understand and apply simulation tools for solving chemical reaction engineering problems, including commercial software for solving chemical engineering problems (detailed knowledge of computer coding is not required).
  LO13 Be aware of the issues involved in obtaining chemical feedstocks and their conversion to chemical products, through the exploration of a number of industrial processes.

  Skills

  Learners are expected to demonstrate the following on completion of the module:
  Core chemical engineering skills in thermodynamics and reaction engineering
  Critical thinking and analysis skill.
  Simulation and modelling skills
  Presentation and communication.

  Coursework

  50%

  Examination

  50%

  Practical

  0%

  Credits

  30

  Module Code

  CHE3101

  Teaching Period

  Full Year

  Duration

  24 weeks

  Pre-requisite

  No

  Core/Optional

  Core

  Chemical Engineering Design Project (50 credits)

  ×

  Chemical Engineering Design Project

  Overview

  Staff:
  Dr. Robin Curry
  r.curry@qub.ac.uk Semester 2
  Dr Chirangano Mangwandi
  c.mangwandi@qub.ac.uk Semester 1
  Dr Danai Poulidi
  d.poulidi@qub.ac.uk Semester 1 & 2
  Dr Chunfei Wu
  c.wu@qub.ac.uk Semester 1 & 2
  Dr Efrosyni Themistou Semester 1
  Dr Bo Xiao b.xiao@qub.ac.uk Semester 1
  Dr Nicole Gui Semester 1
  
  
  Special Requirements:
   1. Presentation and Interviews (week 20, 32): In week 18 students will have an individual interview; this will focus on their chemical engineering design, but will include questions from the all the first semester sections. In week 32 students prepare a group presentation summarising their project to present and discuss in front of a panel of two academic members of staff.
   2. Peer/Self-Assessment (Week 32): Students are required to complete and submit a peer/self-assessment form to their respective project supervisors.
  
   Details on all coursework will be given out in the form of a section brief during term time. – All coursework must be submitted electronically via CANVAS in the format specified in the section brief.
  
   Report Presentation Guidelines:
   Each section must be typed (or if hand calculations / drawings are necessary, these should be scanned) and presented as a single electronic document in MS Word or PDF format. Please ensure that all members of the group follow the same formatting (e.g. font, font size, borders, numbering, etc.). Each section should clearly indicate the person(s) responsible for the work. Each individual section should contain an introduction and conclusion. Details on all report contents will be given in due time as part of each section brief.

  Learning Outcomes

  On completion of this module a learner should be able to:
   Develop skills for design and development of chemical engineering production processes and to carry out design procedures on an existing plant design brought up to the process flow diagram stage. By the end of this module, the student will:
  
   Know and understand the various stages involved in the design of a chemical process;
   Develop the confidence to make decisions on process route selection based on limited information;
   Be able to carry out a heat and mass balance on a complete chemical process with limited information;
   Develop the ability to source the information needed for chemical process design;
   Be able to perform detailed design of chemical engineering equipment;
   Be able to cost a major project with limited information and understand the criteria for project appraisal;
   Be able to develop a control strategy for a chemical process;
   Understand the importance of project management;
   Have developed project management skills;
   Have developed the ability to perform critical path analysis on a large project to optimise resource usage;
   Understand the various steps involved in the design of a chemical process;
   Be able to carry out basic mechanical design of process equipment;
   Understand and apply the key criteria for site selection;
   Conduct an overall assessment of energy flows and perform a pinch analysis of the plant.
   Be able to carry out an assessment of environmental aspects and sustainability of chemical processes;
   Be able to conduct a comprehensive assessment of safety aspects in a chemical process and introduce appropriate safety measures, equipment and procedures;

  Skills

  Skills acquired with module:
  
  The application of cost estimation, control, safety and hazard analysis techniques to a chemical process plant. Detailed chemical engineering design of a specific plant item. In addition, the students will develop group working, project management, leadership, report-writing and presentation skills.

  Coursework

  100%

  Examination

  0%

  Practical

  0%

  Credits

  50

  Module Code

  CHE3104

  Teaching Period

  Full Year

  Duration

  24 weeks

  Pre-requisite

  No

  Core/Optional

  Core

  Transport Phenomena (10 credits)

  ×

  Transport Phenomena

  Overview

  Staff:
  Dr. CM Contribution: 15 Lectures, 8 Tutorials/Seminars.
  
  Dr. BX 9 Lectures, 4 Tutorials/Seminars.
  
  
  DETAILED SYLLABUS – LECTURES (36 hours):
  
  
  1. Differential Analysis (9)
  Lecturer: Dr. Bo Xiao. Room LG439 e-mail: b.xiao@qub.ac.uk
  
  1.1 Time- dependent flow of Newtonian fluids: flow near a wall suddenly set in motion; unsteady Laminar flow between two parallel plates.1.2 Heat transfer: temperature distributions with more than one independent variable;1.2.1 unsteady heat conduction in solids;1.2.2 steady heat conduction in Laminar incompressible flow: 1.2.3 steady potential flow of heat in solids; boundary layer theory for nonisothermal flow.1.3 Diffusivity and the mechanisms of mass transport;1.3.1 Fick’s law of binary diffusion (molecular mass transfer) 1.3.2 mass and molar transportation by convection; 1.3.3 impact of temperature and pressure on diffusivities; 1.3.4 diffusion with a heterogeneous chemical reaction;1.3.5 diffusion with a homogeneous chemical reaction; 1.3.6 gas absorption: diffusion into falling liquid film; 1.3.6 diffusion and chemical reaction inside a porous catalyst.
  
  2. Numerical analysis of Transport Phenomena Systems (7)
  Lecturer: Dr. C. Mangwandi Room LG437 e-mail: c.mangwandi@qub.ac.uk
  
  2.1 Introduction to CFD 2.2 Applications of CFD 2.2.1 Fluid flow in simple geometry 2.2.2 Problems involving mass transport in simple geometries 2.2.1 Reactions engineering models in simple geometry
  3. Transportation of Solids (5)
  Lecturer: Dr. C. Mangwandi Room LG437 e-mail: c.mangwandi@qub.ac.uk
  
  3.1 introduction 3.2 Dilute Phase transport systems 3.3. Dense Phase Transport system 3.2 3.3 Design of Dilute Pneumatic transport systems
  4. Transportation of Slurries (3)
  Lecturer: Dr. C. Mangwandi Room LG437 e-mail: c.mangwandi@qub.ac.uk
  
  4.1. Flow behaviour of slurries 4.2. Pressure drop prediction for slurries 4.3 Heterogeneous slurries 4.4 Components of slurry flow system 4.4 Design slurry transport systems
  
  TUTORIALS/SEMINARS (12 hours):
  
  The students are provided with tutorials, worked examples of the above lecture materials. Tutorials/seminars are an integral element of the module.
  
  1. Differential Analysis (4 hours + 1 HW) - Dr. BX
  2. Non-Newtonian Technology (8 hours + 2 HW) -Dr. CM

  Learning Outcomes

  Students develop competency in the understanding of the theory and application of transport phenomena and non-Newtonian technology. By the end of the module the students will have:
  
  • Understood the analysis of transport processes by means of momentum, mass and energy transport;
  • Appreciated the unifying principles of transport processes in engineering by the similarity of the defining equations;
  • Developed methodologies for solving complex transport problems by analogy;
  • Understood the fundamentals of rheology;
  • Developed complex design problem solving skills and abilities to apply these to the practices involving Newtonian and non-Newtonian fluids.

  Skills

  Skills acquired with module:
  • Analytical and computational skills
  • Critical thinking skills required to solve problems in industrial applications involving fluid flow.

  Coursework

  20%

  Examination

  80%

  Practical

  0%

  Credits

  10

  Module Code

  CHE3004

  Teaching Period

  Full Year

  Duration

  12 weeks

  Pre-requisite

  No

  Core/Optional

  Core

  Mass and Heat Transfer II (20 credits)

  ×

  Mass and Heat Transfer II

  Overview

  STAFF
  
  NAME CONTRIBUTION
  Jehad Abu-Dahrieh j.abudahrieh@qub.ac.uk
  Humidification (13 lectures + 3 tutorials) ;
  Dr Nicole Gui m.gui@qub.ac.uk
  Evaporation (6 lectures + 2 tutorials );Leaching and washing (6 Lectures + 2 tutorials); Drying (6 lectures + 2 tutorials); Crystallisation (4 lectures + 2 tutorials); Membrane processes (7 lectures + 3 tutorials)
  Dr Bo Xiao b.xiao@qub.ac.uk
  Module Co-ordinator
  Multi-component distillation (13 Lectures + 3 tutorials)
  
  Content:
  Lectures (55 Hours):
  Humidification (13 lectures + 3 tutorials):
  Fundamentals of humidification: basic definition; wet-bulb temperature; adiabatic saturation;
  Humidity data for air-water system: temperature-humidity chart; enthalpy-humidity; chart; Mixing of two streams of humid gas; addition of liquid or vapour to a gas.
  Methods for humidification and dehumidification and industrial applications;
  Water cooling: fundamental principle; classification and structure; Design of cooling tower: heat and mass transfer: equilibrium and operating lines; stage calculations; Baker's graphical method; Numerical integration; Carey-Williamson method; packing height calculation; change in air condition; Temperature and humidity gradients in a water cooling tower; Evaluation of heat and mass transfer coefficients. Cooling tower operation and industrial applications.
  Evaporation (6 lectures + 2 tutorials):
  Introduction to evaporation.
  Heat transfer in evaporators: heat transfer coefficient; boiling point rise (BPR); boiling at a submerged surface; forced convection boiling. Single-effect evaporators.
  Multiple-effect evaporators: general heat transfer; calculation and comparison of forward and backward feeds; effect of feed system on economy.
  Improved efficiency in evaporation.
  Evaporator operation.
  Equipment for evaporation: evaporator selection; evaporators with direct heating; natural circulation evaporators; forced circulation evaporators; film-type evaporators; plate-type evaporators; flash evaporators.
  Multi-Component Distillation (13 Lectures + 3 Tutorials):
  Introduction
  Separation sequence; selection of the key components.
  Shortcut methods for multicomponent multistage separations:
  (1) Fenske equation and calculate the minimum equilibrium stages and product distribution;
  (2) Underwood equations for calculation of minimum reflux (Case I & II);
  (3) Gilliland correlation for determination of actual reflux ratio and equilibrium stages
  Equilibrium –Based methods for multicomponent distillation: Theoretical model for an equilibrium stage; MESH equations; Bubble-point (BP) method, Sum-rates (SR) method, and Newton-Raphson (NR) and Inside-Out methods for solving a tridiagonal-matrix equation; Equation-Tearing Procedures Using the Tridiagonal-Matrix Algorithm
  Inside-Out Methods
  Leaching and washing (6 Lectures + 2 tutorials):
  Introduction of leaching and washing: general principle; industrial applications; factors influencing the rate of extraction; mass transfer in leaching operation;
  Equipment for leaching: extraction from different materials; batch extractors; continuous extractor; continuous, counter-current washing.
  Calculation of the number of stages: equilibrium-stage model for leaching and washing; McCabe-Smith Algebraic methods; variable underflow.
  Rate- based model for leaching: food processing; mineral processing.
  Drying (6 lectures + 2 tutorials)
  Introduction to drying.
  Moisture-solid relationships; Mass and enthalpy balances.
  Types of moisture.
  Hygroscopicity.
  Drying rate curves; The constant drying rate period; Critical moisture content.
  Fall rate periods.
  Movement of moisture within a solid through drying.
  Total drying time.
  Rotary dryers; Drying equipment.
  Crystallisation (4 lectures + 2 tutorials):
  Introduction of crystallization.
  Growth and properties of crystals: saturation, nucleation, growth of crystals, effect of impurities on crystal formation, effect of temperature on solubility, fractional crystallization, caking of crystals and yield of crystals.
  Crystallizers: batch and continuous crystallizers; industrial applications.
  Membrane Processes (7 Lectures + 3 Tutorials):
  Introduction to membrane processes.
  Classification of membrane processes.
  Brief summary of membrane structure and types of membranes.
  Principle of operation of membrane separation units.
  Fundamental aspects of membrane processes; flux equations; mass transfer relationships; permeation rate; pressure drop relationships.
  Brief review of membrane applications.
  Electrically augmented membrane separation processes.
  The concept of concentration polarisation.
  The electro-kinetic flux equations.
  Electroceramic membranes and applications.
  Detailed Syllabus – Tutorials/Seminars (17 Hours):
  Students are provided with tutorial and worked examples of the above lecture material. Tutorial classes are an integral element of the module.
  
   1. Humidification (3 tutorials), JAD
   2. Evaporation (2 tutorials), NG
   3. Multi-phase distillation (3 tutorials), BX
   4. Leaching and washing (2 tutorials), NG
   5. Drying (2 tutorials), NG
   6. Crystallisation (2 tutorials), NG
   7. Membrane processes (3 tutorials), NG
  
  Coursework: to pass this module students have to complete two quiz/class tests on membrane processes and drying.

  Learning Outcomes

  On completion of this module a learner should be able to:
  Students are expected to understand the fundamentals and principles of heat and mass transfer. Students will develop competency in solving problems in humidification, drying, membrane, evaporation, distillation and crystallisation processes by applying fundamental concepts and principles of heat and mass transfer.
  By the end of the module the students will:
  Appreciate the development of analysis skills in the fundamental aspects of heat and mass transfer;
  Build up practical knowledge about the industrial use of heat and mass transfer in humidification, drying evaporation and crystallisation and membrane separation and understand this processing classification and associated technical criteria.
  Develop the ability to apply fundamental heat and mass transfer theories to design.
  Be able to apply approximate and rigorous methods of distillation to solve separation problems involving multi-components.

  Skills

  To develop skills of applying simultaneous heat and mass transfer principles in the design of cooling towers, membrane, dryers, distillation and evaporators.

  Coursework

  20%

  Examination

  80%

  Practical

  0%

  Credits

  20

  Module Code

  CHE3102

  Teaching Period

  Full Year

  Duration

  24 weeks

  Pre-requisite

  No

  Core/Optional

  Core

• Year 4

  Core Modules

  Green Chemical Engineering (10 credits)

  ×

  Green Chemical Engineering

  Overview

  Staff: Dr. H. Manyar Contribution: 24 Lectures, 12 Coursework.
  
  DETAILED SYLLABUS – LECTURES (24 hours):
  
  Sustainability and Chemical Industry (16)
  
  1.1. Review of Sustainability, 12 Principles of Green Chemistry, E-Factor, Atom Economy 1.2. Role of Chemical Industry in Sustainable development 1.3. Criteria for Benign process design 1.4. Resource conservation and Waste reduction 1.5. Sustainable Resource management (water, air, carbon balance, feedstocks) 1.6. Sustainable waste management 1.7. Renewable chemicals from cellulose, hemicellulose and lignin 1.8. Biorefinery products 1.9. Case studies, (i) Amide synthesis, Grignard vs Beckmann rearrangement (ii) renewable paracetamol (iii) Ibuprofen synthesis (iv) Friedel-Crafts Alkylation (v) PETE vs PEF, biodegradable plastics.
  
  Sustainable Chemicals Production/ Factories of Future (8)
  
  2.1. Traditional chemical processes vs more recent development 2.2. Small modular, flexible chemicals production 2.3. Case studies using micro-reactors, induction-heating, sono-chemical, photo-chemical, microwave reactors, modular plants, lab-on-a-chip, Plant-on-a-truck.
  
  DETAILED SYLLABUS –Coursework (12 hours):
  
  The students are provided with tutorial, worked examples and case studies of the above lecture material. Tutorial and workshops are an integral element of the module.
  
  Coursework assignments:
  
  Green Chemical Process Design Project
  
  This assignment will provide an opportunity to work in group of 4-5 students each. The project work consists of technical evaluation of a traditional chemical process, on the basis of 12 principles of industrial and green chemistry and propose a greener chemical process by using alternative routes and better chemical engineering process design. The group will prepare a project report of 10-15 pages to be submitted at the end of the semester (20%). Suggested format for the report is 1.5 spacing, Calibri, 11 font size including cover page, group contribution breakdown; table of contents, summary, introduction, comparison of traditional and proposed greener route on the basis of mass and energy balances, references and appendix.
  
  Workshop based on GREENSCOPE
  
  In this workshop, students will be using GREENSCOPE, which is a tool developed by US EPA. GREENSCOPE is a multi-objective process evaluator, which can be used to measure the sustainability of any process. On the basis of which new chemical process or modifications to existing process could be proposed. Students will work in groups of 4-5 each, preferably on the process of their choice.

  Learning Outcomes

  At the end of the module the students are expected to develop awareness about the essential role of engineering green chemical processes to achieve sustainable development and reduced emissions. By the end of the module the students will have:
  
  LO1: understand the importance of sustainability in the context of chemical manufacturing
  LO2: develop skills to measure the green process metrics, E-factor, atom economy
  LO3: critically evaluate and compare the greenness of chemical processes
  LO4: analyse and interpret the impact of chemical processes on the environment and society by application of principles of green chemical engineering.
  LO5: develop strategies for engineering green & sustainable chemical processes by intensification of processes and minimization of waste generated.
  LO6: understand life cycle assessment and carbon footprint
  LO7: awareness of sustainable waste management and add-value to waste by valorization of resources
  LO8: apply knowledge of green engineering to design sustainable chemical processes
  LO9: awareness of future chemical production technologies & modern developments in chemical plant design

  Skills

   STEM – Core skills in underlying physics, chemistry and math are applied to solving problems including mass and energy balances, efficiency calculations and economic evaluation.
   Critical thinking skills – Students can critically evaluate different options and present thought through analysis of chemical processes.
   Analytical – Evaluation of data and its use.
   Communication – discussion of important factors and the presentation of data including written reports.
   Learning and management - Improving independent learning and time management.

  Coursework

  30%

  Examination

  70%

  Practical

  0%

  Credits

  10

  Module Code

  CHE4107

  Teaching Period

  Full Year

  Duration

  12 weeks

  Pre-requisite

  No

  Core/Optional

  Core

  Advanced Topics in Chemical Engineering (20 credits)

  ×

  Advanced Topics in Chemical Engineering

  Overview

  STAFF:
  NAME CONTRIBUTION
  Lorenzo Stella (l.stella@qub.ac.uk)
  Numerical Methods for Chemical Engineering Applications
  Peter Robertson (p.robertson@qub.ac.uk)
  Artificial Photosynthesis
  Nathan Skillen (n.skillen@qub.ac.uk) Artificial Photosynthesis
  Chirangano Mangwandi (c.mangwandi@qub.ac.uk)
  Agglomeration and Granulation; module coordinator
  Chris Murnaghan (c.murnaghan@qub.ac.uk)
  Biopharmaceutical Engineering
  Dr Daniel McStay (daniel.mcstay@inov8s.com)
  Technology Management and Entrepreneurship
  Prof David Rooney (d.rooney@qub.ac.uk)
  Technology Management and Entrepreneurship
  
  This module is comprised of a compulsory numerical methods component (5 CATS), in addition to five further optional components, each weighted at 5 CATS points, of which students select three to study within the module. Further information in relation to each of the module topics is provided below.
  
  Numerical Methods for Chemical Engineering Applications (Compulsory)
  This submodule builds on B-level mathematical and programming skills with MATLAB©. In the first part of the submodule, the student will gradually develop a MATLAB© script to fit complex reactions models using the least squares method. The first assignment includes a discussion of the quality of the fit against an existing benchmark. In the second part, the students will progressively build a numerical model of a realistic model of a packed bed reactor COMSOL© Multiphysics© which includes both the details of complex reaction-diffusion of multiple species in the pellets and the pressure drop in the bulk phase. The second assignment includes a discussion of the relevance of non-isothermal conditions in the reactor.
  
  Lecture Topics:
  • Fitting a complex reaction model using the least squares method
  • Example of a MATLAB® implementation of the least squares method
  • Revision of Partial Differential equations (PDEs) in Chemical Engineering and their solution using the Finite Element Method (FEM)
  
  Workshop Topics:
  • Solving stationary reaction-diffusion equations (heterogeneous catalysis) with realistic boundary conditions using COMSOL®.
  • Example of catalyst pellets with multiple reactions and mass transfer limitations.
  • Solving stationary non-isothermal reaction-diffusion problems (Weisz-Hicks method) with COMSOL®.
  • COMSOL® multiphysics modelling of a packed bed tubular reactor.
  • Example of coupled mass (reaction-diffusion equation) and momentum (Ergun equation) transfer.
  • Adding heat transfer to the model. *If time permits
  
  NOTE - Assessment:
  This topic is assessed via continual assessment, consisting of:
  
  1. Assignment 1 - MATLAB model fitting with the least squares method
  2. Assignment 2 - COMSOL® modelling of a packed bed reactor
  
  Additionally, submission of materials related to workshops for this topic is compulsory, however, no marks
  are awarded for those elements.
  
  Artificial Photosynthesis (Optional)
  Solar energy is converted to a potential food stock, specifically through conversion of atmospheric CO2. Over the past 50 years there have been considerable efforts put into the development of artificial photosynthetic systems to convert CO2 to useful energy products. This has included the development of novel materials and devices that can harvest solar energy for conversion to renewable fuels. Subject to the development of technologically and economically viable processes there is huge scope for this process through the utilization of solar energy to convert both water and CO2, two abundant raw materials, to renewable fuel products and hence address the looming global energy challenges. This sub-module will focus on the various approaches to developing artificial photosynthetic systems and consider the current state of the art in terms of research and technology.
  Lectures:
  1. Introduction to Artificial Photosynthesis
  2. Natural Photosynthesis 1
  3. Natural Photosynthesis 2
  4. Bio-inspired Systems/The Death of Biofuels?
  5. Artificial/Bionic Leaf
  6. Artificial Photosynthesis of Hydrogen
  7. Reduction of Carbon Dioxide via Artificial Photosynthesis
  8. Waste Materials/Biomass and Artificial Photosynthesis
  9. Molecular Sensitisers for Artificial Photosynthesis
  10. Measuring Yields and Efficiencies of Artificial Photosynthetic Processes
  11. Dark Reactions and a Numbers Game
  12. Upscaling of Artificial Photosynthetic Processes
  A workshop will also be delivered within this topic in relation to the aspects listed above.
  
  Agglomeration and Granulation (Optional)
  Size enlargement unit operation is used in several industries such as food, pharmaceutical and agricultural, to process powder material into products with better flow and handling properties and improved functionality. The objective of this sub-module is to introduce granulation and agglomeration size enlargement techniques.
  Lectures:
  1. Introduction to powder processing
  2. Introduction to size enlargement
  3. Wet Agglomeration Techniques
  4. Dry granulation Techniques
  5. Granulation rate process
  6. Modelling of size enlargement process
  Workshops:
  1. Size Analysis
  2. Modelling Solid Systems with ASPEN
  Tutorials will also be delivered within this topic in relation to the aspects listed above.
  
  Biopharmaceutical Engineering (Optional):
  Biopharmaceutical engineering is a branch of engineering focused on the discovery, formulation, and manufacture of biopharmaceuticals, as well as analytical and quality control processes, which ensure the safety of the end user. This area involves the study and understanding of a wide range of areas including bio/chemistry, chemical engineering, biomedical engineering, and pharmaceutical sciences.
  This course will provide students with an understanding of the principal scientific and engineering challenges involved in the development and manufacture of biopharmaceuticals, in addition to aspects of the design, operation and management of biopharmaceutical production facilities.
  Lectures:
  1. Changing Nature of the Pharmaceutical Industry: Small to Large Molecules
  2. Physical Chemistry & Engineering Principles in Drug Dissolution and Classification
  3. Formulation and Delivery of Biopharmaceuticals
  4. Designing Cell Factories
  5. Separation of Biopharmaceuticals 1
  6. Separation of Biopharmaceuticals 2
  7. Characterisation of Biopharmaceuticals
  Workshops/Seminars:
  1. Facility Design, Operation and Management, Bio/Pharmaceutical Industry Regulation and QC
  
  Directed Self-Study:
  1. Basics of Molecular Genetics & Biotechnology
  2. Biopharmaceutical Drug Discovery
  3. Drug delivery systems
  4. Lean Six Sigma
  
  Technology Management and Entrepreneurship (Optional)
  Many chemical engineers will progress into senior management positions and as they do their skill sets need to adjust to include wider business acumen. This topic is designed to enhance knowledge of creativity, leadership and business practice. The topic is delivered through four interlinking themes each of which include pre/post-reading material and live workshops. These four themes are:
  1. Creativity and design thinking
  2. Innovation management
  3. Leadership and people
  4. Financing and growth

  Learning Outcomes

  For the extensive learning outcomes please see the full synopsis on CANVAS

  Skills

  On completion of the module, students are expected to be able to demonstrate a range of skills, dependent on the optional topics selected, including:
  
  Numerical Methods for Chemical Engineering Applications:
  • Advanced modelling and computer programming
  • Written presentation skills
  • Independent and group learning
  
  Artificial Photosynthesis:
  • Ability to select appropriate photosensitising materials for artificial photosynthesis applications and
  • Skill in critical assessment of artificial photosynthetic systems as alternative energy processes
  • Ability to undertake economic and technical analysis of system efficiency
  • Skills to select of key reactor design parameters for various artificial photosynthetic processes
  
  Agglomeration and Granulation:
  • Problem solving skills in relation to particle sizing
  • Designing of systems for processing and handling of particulate products
  • Analysis of bulk movement of particulate product
  
  Biopharmaceutical Engineering:
  • Design, operation, management of biopharmaceutical reactors
  • Analysis and characterisation of biopharmaceuticals
  • Design of systems in line with regulatory legislation relating to biotechnological products
  
  Technology Management and Entrepreneurship:
  • Skills in innovation, entrepreneurship and quality management
  • presentation, leadership
  • self-awareness and communication

  Coursework

  25%

  Examination

  75%

  Practical

  0%

  Credits

  20

  Module Code

  CHE4102

  Teaching Period

  Full Year

  Duration

  24 weeks

  Pre-requisite

  No

  Core/Optional

  Core

  Energy Systems: Oil and Gas to Renewables (20 credits)

  ×

  Energy Systems: Oil and Gas to Renewables

  Overview

  Staff:
  Prof D Rooney Contribution: 12 Lectures, 6 Workshops
  Prof P Robertson Contribution: 12 Lectures, 6 Workshops
  Dr. C Wu Contribution: 12 Lectures, 6 Workshops
  Industry speakers Contribution: 18 Workshops
  
  
  DETAILED SYLLABUS – LECTURES (24 hours):
  
  1. Introduction to the modern oil and gas sector (1 hour)
  2. Thermodynamics of Oil and gas reserves (3 hours)
  3. Downstream and upstream separation technologies (5 hours)
  4. Energy transitions in the Oil and gas sector (3 hours)
  5. Introduction to Renewable Energy systems (2 hours)
  6. Biomass and Biofuels (1 hour)
  7. Modern renewable energy technologies (5 hours)
  8. Energy recovery and storage (4 hours)
  9. Environmental impacts of energy (1 hour)
  10. Renewable energy in transport systems (2 hours)
  11. Future cities (1 hour)
  12. Introduction of biomass gasification (2 hours)
  13. Tar reduction from biomass gasification (2 hours)
  14. Carbon capture using solid sorbents (2 hours)
  
  
  DETAILED SYLLABUS – Workshops and Coursework (36 hours):
  
  The students are provided with project work related to the learning outcomes of the module. Workshops will focus on the core themes listed below. These workshops will facilitate project work and is supported by reading and other online resources to support the discussion.
  
  1. Thermodynamic model construction and use (6 hours)
  2. Designing renewable energy systems (3 hours)
  3. Future transport systems (3 hours)
  4. Photovoltaic systems (6 hours)
  5. Biomass handling (3 hours)
  6. Agricultural emission abatement (3 hours)
  7. Towards achieving a zero carbon economy (3 hours)
  8. Regional Energy transitions (6 hours)
  9. Leadership in the energy sector (3 hours)

  Learning Outcomes

  At the end of the module the students are expected to be able to:
  
  Understand the evolving role of Oil & Gas Companies in the context of global energy systems
  Describe the technologies and underpinning engineering/science associated with modern Oil, Gas & Petrochemical facilities (upstream and downstream)
  Critically evaluate various forms of renewable energy including wind, marine, solar geothermal and biomass
  Explain key decision factors in choosing appropriate energy systems
  Analyse and interpret data sets for energy trading
  Apply advanced thermodynamic modelling techniques to areas including multi-phase hydrocarbon streams and waste heat recovery systems.
  Understand current and emerging conversion routes for biomass and evaluate the related challenges towards their deployment.
  Apply knowledge of renewable energy systems to the design of future buildings, cities and transport infrastructure.

  Skills

  STEM – Core skills in underlying physics, chemistry and math are applied to solving problems relevant to energy systems.
  Critical thinking skills – Students can critically evaluate different options and present thought through analysis of energy systems.
  Analytical – Evaluation of data and its use.
  Communication – discussion of important factors and the presentation of data including written reports.
  Learning and management - Improving independent learning and time management.

  Coursework

  100%

  Examination

  0%

  Practical

  0%

  Credits

  20

  Module Code

  CHE4105

  Teaching Period

  Full Year

  Duration

  24 weeks

  Pre-requisite

  No

  Core/Optional

  Core

  Research Project (40 credits)

  ×

  Research Project

  Overview

  DETAILED SYLLABUS
  
  Facilitation of research practice
  Within this module, students will carry out a research project under the supervision of an academic and/or industrial supervisor, within an applied area of Chemical Engineering. Students participating within this module will be required to undertake a significant amount of research activity as part of their timetabled activities across both semesters 1 and 2.
  
  Assessment structure
  Assessment within this module will constitute three main themes, each of which will assess students’ skills and abilities within key aspects of research activity. These themes, along with their associated assessments, are outlined below.
  
   
  Theme 1. Project feasibility and introduction (20% of module assessment)
  Students will be required to submit a document consisting of two main components:
  
  • A feasibility study related to the research project, not exceeding 3000 words (excluding title pages and references) (100% of the theme mark)
  • A literature review of the related research area, not exceeding 2000 words (excluding title pages and references)
  
  Notes: Assessment of submissions will take place early in Semester 2, with feedback subsequently being provided via a student-supervisor meeting. Attendance at this feedback meeting is compulsory, and will be arranged with you, via email, by your academic supervisor.
  
  An amended version of the literature review component of the project feasibility and introduction report is expected to constitute the introduction of the final project thesis which is to submitted later in Semester 2, and as such, will not be assessed as part of Theme 1 – rather, this submission will allow students to receive structured feedback before the assessment of this material within the final submitted research thesis. It is however essential that a suitable literature review is conducted so as to properly inform the feasibility study element, and to facilitate the provision of adequate feedback.
  
  
  Theme 2. Dissemination of data (60% of module assessment)
  This theme will be assessed across three submissions:
  
  1. Research thesis (50% of theme mark) – this final report, not exceeding 8000 words (excluding title pages and references), will be assessed by both the supervisor and an assigned second marker, with an average of the awarded marks being used to assign the final mark for the report. This report must take an orthodox structure, with guidance being provided by the project supervisor. Where marks awarded by assessors deviates by more than 5%, the report will be further assessed by a third independent assessor.
  
  2. Poster presentation (20% of theme mark) – students are required to prepare and present a poster presentation, of A0 size (landscape orientation, 118.9 cm x 84.1 cm) which will be assessed by two assigned academic markers (not including your academic supervisor), with an average of the awarded marks being used to assign a final mark for the poster presentation.
  
  3. Viva voce examination (30% of theme mark) – students will be required to attend a 15-minute oral examination, consisting of two sections, namely a five-minute oral presentation, and ten minutes of questioning/discussion from the academic panel made up of two allocated members of academic staff (not including your academic supervisor). An average of the marks awarded by each of the panel members will be used to assign a final mark for the viva voce examination.
  
  
  
  
  
  
  Theme 3. Experimental records (20% of module assessment)
  This theme consists of two assessments:
  
  1. Data collection and communication of results (75% of theme mark) – students will be required to submit their experimental records (including lab books, and electronic copies of supplementary data, where appropriate), which will then be assessed by the academic supervisor and an assigned second assessor, who will consider two main aspects:
  
  • Use and maintenance of experimental records, including quality of results and level of work conducted
  • Application of results, including how data has been utilised to construct components which have been provided within other assessed aspects
  
  An average of the marks awarded by each assessor will be used to assign a final mark for this aspect of assessment.
  
  It is critical that students clearly and unambiguously identify their own work within their records. Any work which was shared by or with another student or researcher must be marked as such to avoid collusion or plagiarism investigations taking place, in line with University regulations.
  
  2. General overall performance (25% of theme mark) – the academic supervisor will provide an assessment of students’ overall performance throughout the project, with this assessment to include aspects relating to behaviour within the research environment, engagement with the research project, etc.
  
  
  Assignment Submission
  The following report documents must be submitted online, via Canvas, using the system’s assignments functionality:
  
  • Theme 1 report
  • Research thesis
  
  Please note that each of these submissions will be processed using the University’s originality checking system, in order to ensure that submitted work has not been plagiarised. Students must be aware of the University’s regulations in relation to plagiarism, in addition to other forms of academic offence, and ensure that these are considered ahead of submitting their work.
  
  There is no requirement to submit documents relating either the poster presentation or oral presentation components of the module, as these aspects will be assessed in their entirety, during the delivery of the particular presentation. Students are, however, responsible for the production and availability of presentation resources at the time of assessment – this includes the printing and display of poster presentations in a timely manner, and the provision of presentation slides, if required, during the viva voce examination.
  
  Further submitted work, including lab books and supplementary electronic data, must be physically submitted – further details of the submission process for these elements will be provided a sufficient amount of time in advance of the submission deadline. Further, students should ensure that electronic data is provided in a standard portable data format (i.e. a USB-compatible device). Please note that any alternative form of laboratory notes, apart from the actual original physical copies of these components, will not be accepted.
  
  Deadlines
  Deadlines for each of the detailed assessment components above, in addition to details relating to poster presentation and viva voce examination sessions will be provided, in due course, via assignment briefing information provided on Canvas, by the module coordinator. Students are reminded that it is their responsibility to be fully aware of such deadlines. Late submissions will be penalised in line with the appropriate University regulations, to a maximum deduction of all marks.
  
  Students should note that the submission of ALL assessed components is COMPULSORY.
  
  Assessment criteria
  Assessment criteria for each component of assessment within this module are provided within the appendices at the end of this document – students are encouraged to ensure that they are fully aware of these, referring to them regularly as they complete their work, ensuring that queries/concerns about these aspects are discussed with their academic supervisor where necessary.
  See CHE4012 on Canvas for detailed Appendices.

  Learning Outcomes

  On successful completion of this module, students will have:
  
  • Carried out an advanced research project within an applied area of Chemical Engineering, commensurate with professional research standards
  • Carried out a significant level of consultation with, and critical analysis of research and commercial literature, and/or other appropriate data sources
  • Developed an advanced level of understanding in relation to feasibility assessment of research and development projects
  • Designed and implemented novel research approaches, via the application of theoretical knowledge and problem-solving skills
  • Successfully planned and delivered a research proposal
  • Demonstrated notable competence in experimental and/or computational techniques needed to generate new findings
  • Shown proficiency in collection, validation, and analysis of research data
  • Carried out complex mathematical and/or statistical analysis of research data, and reported the methodology and results obtained
  • Effectively communicated background information and research outcomes at a professional level via formal written reports, poster presentations, and oral routes
  • Developed skills in working with academic and/or industrial research teams
  • Demonstrated a high-level understanding of a key research area within Chemical Engineering, including an awareness of the current state of the art
  • Provided evidence of significant experience, knowledge, and expertise in the identification of risks within laboratory/engineering working environments, and implemented safe working practices, via awareness of appropriate health and safety legislation 

  Skills

  On successful completion of this module, students will have gained a range of skills, including, but not limited to:
  
  • Location and utilisation of academic and other applicable types of literature
  • Practical/experimental research
  • Effective utilisation of sophisticated laboratory equipment
  • Project planning and time management
  • Critical thinking
  • Problem solving
  • Application of theoretical knowledge
  • Independent working
  • Teamworking
  • Safe and healthy working
  • Effective utilisation of software packages, where appropriate
  • Communication and argument construction

  Coursework

  100%

  Examination

  0%

  Practical

  0%

  Credits

  40

  Module Code

  CHE4012

  Teaching Period

  Full Year

  Duration

  24 weeks

  Pre-requisite

  No

  Core/Optional

  Core

  Advanced Chemical Reaction Engineering (20 credits)

  ×

  Advanced Chemical Reaction Engineering

  Overview

  STAFF
  
  NAME CONTRIBUTION
  Dr Nancy Artioli.
  n.artioli@qub.ac.uk Contribution: 27 hrs Lectures: Heterogeneous catalytic reactions.
  Dr Lorenzo Stella l.stella@qub.ac.uk Contribution: 9 hrs Lectures, 4 hrs Computer Workshops: Modelling transport and reaction in a catalytic filter.
  Dr Claire McAtee
  c.mcatee@qub.ac.uk Contribution: 10 hrs workshops.
  
  
  
  Course Summary:
  The course will cover the advanced aspects of kinetics, data acquisition, data interpretation, heterogeneous catalysis, and heat and mass transfer. The students will acquire knowledge about different heterogeneous catalysis for environmental protection and they will be able to apply chemical engineering principles to model kinetic behaviour of catalytic system for exhaust gas cleaning.
  The course will be taught partly by means of examples from research, showing how the basics of catalysis, advanced catalyst preparation, catalyst characterization and modelling are used to understand and develop catalytic systems in this field.
  
  Prerequisites:
  This course builds on previous content covered throughout your degree to date. As such, the course team has an expectation of prior learning outcomes being met from earlier modules. More specifically, the course team expects B-level mathematical skills, including confidence with differential and integral calculus, matrix and vector operations, solutions of ordinary differential equations, partial differentiation basics programming skills with MATLAB, 2D and 3D data visualisation, B-level competence in thermodynamic principles, catalysis, chemical reactions, reactor design, reaction equilibrium, application of chemical reaction engineering principles and development of catalytic reactor model and designs, application of kinetic equations to the design of reacting systems based on CHE2105 and CHE3101.
  
  Module content:
  Heterogeneous catalytic reactions:
  • Basic introduction into heterogeneous catalysis
  • Preparation of heterogeneous catalysts
  • Characterization of heterogeneous catalysts
  • Exhaust gas catalysis for internal combustion engines: Three-way-catalysis, oxidation catalysts, selective catalytic reduction, NOx storage reduction catalyst, soot filtration/oxidation, methane oxidation, SOx, volatile organic compounds
  • Relevant experiments on the topic emission control, catalyst characterization
  • Development of kinetic modelling: kinetics of heterogeneous catalytic reactions.
  • Derivation of rate expressions.
  • Effects of transport limitations on rates of solid-catalysed reactions: verification of heat and mass transfer limitation.
  • Introduction to monolith reactor modelling: mass, energy and momentum transport.
  • Screening of experimental data and fitting for chemical reactions
  • Model discrimination and statistical analysis.
  
  
  Modelling transport and reaction in a catalytic filter:
  • Full transport equations, including non-ideal flow, reactions, and non-isothermal condition
  • Method of solutions and approximations
  • Finite element method implementation, general aspects
  • Solution of the isothermal 3D model of the wall-through and flow-through catalytic filters using COMSOL® Multiphysics®. Comparison with the simplified 1D model solutions.
  • Full 3D solution of the non-isothermal model of the wall-through and flow-through catalytic filters using COMSOL® Multiphysics®. Comparison with the simplified 1D model solutions.
  
  • Revision

  Learning Outcomes

  On completion of this module a learner should be able to:
  • General learning outcomes:
  • Students will build on and further develop the learning and skills from Level 3 and enhance their knowledge in chemical reactions.
  • Specific learning outcomes:
  • Knowledge, evaluation of current and emerging technologies in catalytic conversion.
  • Design and critical appraisal of a kinetic model for after-treatment devices
  • Further extend their knowledge relating to the use of MATLAB® and COMSOL® Multiphysics® as tools for solving and aiding in chemical reaction problem solving.
  • Further develop their knowledge in reaction kinetics for heterogeneous catalytic reactions.
  • Critical evaluate the important of heat and mass transfer limitation in chemical reactions.
  • Enhance skills in data processing and model development.
  • Further develop their knowledge in solving non-steady state problems for chemical reactions.
  • Enhance skills in numerical methods development

  Skills

  Learners are expected to demonstrate the following on completion of the module:
  • STEM – Core skills in underlying physics, chemistry and math are applied to solving problems including mass and energy balances, efficiency calculations and economic evaluation.
  • Core chemical engineering skills in thermodynamics and reaction engineering
  • Computational and modelling skills
  • Critical thinking skills – Students can critically evaluate different options and present thought through analysis of chemical processes.
  • Analytical – Evaluation of data and its use.

  Coursework

  50%

  Examination

  50%

  Practical

  0%

  Credits

  20

  Module Code

  CHE4109

  Teaching Period

  Spring

  Duration

  12 weeks

  Pre-requisite

  No

  Core/Optional

  Core

  Environmental Engineering Design (10 credits)

  ×

  Environmental Engineering Design

  Overview

  Course delivery.
  Each Project will begin with an Introductory Lecture, followed by a combination of Lectures, scheduled Group sessions (attended by the Lecturer/Section Expert) and independent Group work. All assignments to be submitted electronically via Canvas.
  
  Schedule for Teaching, Continual Assessment and Submission Deadlines.
  
  Week/s, Content and Design project submission deadline/s:
  
  Weeks 1 – 5 Project 1.
  Life Cycle Analysis (LCA) of Biogas/bioenergy systems.
  2 Lectures, 2 hours, Group Sessions, Research and Site Visit to Anaerobic Digestion/Biogas plant. Dr Curry.
  Deadline: End of Week 5. Friday 23rd October.
  
  Weeks 6 - 10 Project 2.
  4 Lectures 4 hours. Introduction to Photocatalytic technologies. Prof Robertson.
  Project 2. Photocatalytic reactor design.
  Group Sessions and Research.
  Prof Robertson.
  Deadline: End of Week 10. Friday 27th November.
  
  Staff:
  Prof. P. Robertson 4 Lectures/Group Sessions
  Dr R. Curry (MC) 2 Lectures/Group Sessions
  
  
  DETAILED SYLLABUS – LECTURES (32 hours):
  
  1. Review of Biogas Systems and Life Cycle Analysis (LCA) of Biogas/Bioenergy systems.
  Lecturers: Dr R. Curry - Room No. LG.013 - Email: r.curry@qub.ac.uk
  
  1.1. Review of Bioenergy content from Levels 1-3 and latest developments. 1.2. Review of LCA principles from L2 and application of LCA to Bioenergy systems. 1.3. Selection and critical evaluation of feedstocks and processes for bioenergy production. 1.4. Analysis and evaluation of Case Studies of the application of LCA to Bioenergy systems. 1.5. Key issues and challenges in application of LCA/CF to bioenergy processes. 1.5. Literature review, technology evaluation and critical review of data sources. 1.6. Development of Life Cycle Inventory (LCI) of feedstocks and processes. 1.7. Development of Model for Life Cycle Analysis (LCA) of Greenhouse Gas (GHG) balances of biogas production and utilisation options. 1.8. Integration of UK GHG Inventory data for electricity and gas production. 1.9. Comparative evaluation of GHG balances for Bioenergy and fossil sources. 2.0. Identification and modelling of innovative technologies for biogas production and utilisation. 2.1. Sensitivity analysis of data and technology performance assumptions.
  
  2. Photocatalytic Technologies.
  Lecturer: Prof. P. Robertson – Room No. 02.424 – Email : p.robertson@qub.ac.uk
  
  2.1. Basic photocatalytic processes. 2.2. Selection and evaluation of photocatalyst materials. 2.3. Introduction to the design principles of photocatalytic reactors. 2.4. Design and construction of immobilised film, fluidised bed and suspended catalyst photoreactors. 2.5. Mass transport and kinetic modelling and control in photocatalytic reactors. 2.6. Irradiation sources and light distribution in photocatalytic reactors. 2.7. Determination of conversion efficiencies, quantum yields and economic evaluation of photocatalytic reactors 2.8. Applications of photocatalytic technology for energy conversion/storage and .treatment of contaminated water and air.

  Learning Outcomes

  General learning outcomes:
  Students will build on and further develop the learning and skills from Level 3 through the design and critical appraisal of current and emerging technologies in environmental and bioengineering.
  
  Specific learning outcomes:
  Knowledge, evaluation, design and critical appraisal of current and emerging technologies in bioenergy.
  Knowledge and understanding of Life Cycle Analysis Inventory and Model development;
  Knowledge, evaluation and design of photocatalytic technologies for environmental remediation and sustainable energy applications.
  Knowledge, evaluation, design and critical appraisal of current and emerging technologies in catalytic conversion.
  
  At the end of the module the students are expected to be able to:
  
  • Describe and critically evaluate photocatalyst materials and processes for both energy conversion/storage and environmental applications;
  • Carry out kinetic and light modelling of photoreactors and critically appraise the outputs;
  • Evaluate and critically appraise the technical and economic feasibility of photocatalytic technologies for both environmental remediation and solar energy conversion and storage;
  • Design, evaluate and critically appraise the photocatalytic reactor configurations for sustainable energy and environmental remediation applications.
  • Demonstrate knowledge and understanding of the principles of Life Cycle Analysis (LCA) and its application to Bioenergy processes and systems;
  • Search and critically evaluate the literature and compile an inventory of technology performance assumptions and associated CO2-eq emissions for the Biogas/Bioenergy production and utilization system;
  • Build an Excel model and apply this to carry out a Life Cycle Analysis of biogas production and utilisation;
  • Identify and carry out LCA modelling of innovative technologies for biogas production and utilisation;
  • Demonstrate knowledge and understanding uncertainty and complexity in inventory development and modelling through the use of Sensitivity Analysis.

  Skills

  Skills acquired with module:
  Knowledge and understanding of current and emerging technologies in environmental and bioengineering.

  Coursework

  100%

  Examination

  0%

  Practical

  0%

  Credits

  10

  Module Code

  CHE4108

  Teaching Period

  Full Year

  Duration

  12 weeks

  Pre-requisite

  No

  Core/Optional

  Core

Entrance requirements

A level requirements

AAA including Mathematics at least one from Chemistry (preferred), Biology, Computer Science, Digital Technology, Geography, ICT (not Applied ICT), Physics, Software Systems Development or Technology & Design.

A maximum of one BTEC/OCR Single Award or AQA Extended Certificate will be accepted as part of an applicant's portfolio of qualifications with a Distinction* being equated to a grade A at A-level.

Irish leaving certificate requirements

H2H2H3H3H3H3 including Higher Level grade H2 in Mathematics and a Science subject (see list under A-level list requirements)

Access Course

Not considered. Applicants should apply for the BEng Chemical Engineering degree.

International Baccalaureate Diploma

36 points overall including 6,6,6 at Higher Level including Mathematics and a relevant Science subject (Chemistry preferred) - see list under A-level requirements.

If Chemistry or Physics is not offered at Higher Level then GCSE Chemistry and Physics grade B/6 or Double Award Science grades BB/66 would be required.

Standard Level grade 5 would be acceptable in lieu of the GCSE requirement.

Graduate

A minimum of a 2:2 Honours Degree, provided any subject requirements are also met.

Note

All applicants must have GCSE English Language grade C/4 or an equivalent qualification acceptable to the University.

Applicants not offering Chemistry or Physics at A-level should have a minimum of either a grade B/6 in GCSE Chemistry and Physics, or GCSE Double Award Science grades BB/6,6.

Further information

Applicants for the the MEng degree will automatically be considered for admission to the BEng degree if they are not eligible for entry to the MEng degree both at initial offer making stage and when results are received.

Option to transfer

Transfers between BEng and MEng may be possible at the end of Stage 2.

How we choose our students

Applications are dealt with centrally by the Admissions and Access Service rather than by the School of Chemistry and Chemical Engineering. Once your application has been processed by UCAS and forwarded to Queen's, an acknowledgement is normally sent within two weeks of its receipt at the University.

Selection is on the basis of the information provided on your UCAS form. Decisions are made on an ongoing basis and will be notified to you via UCAS.

For last year's intake, applicants for MEng degrees in Chemical Engineering offering A-level/BTEC Level 3 qualifications must have had, or been able to achieve, a minimum of six GCSE passes at grade B/6 or better, to include Mathematics (minimum grade C/4 required in GCSE English Language). However, this profile may change from year to year depending on the demand for places. Applicants not offering Chemistry or Physics at A-level require either grade B/6 in GCSE Chemistry and Physics, or grades BB/6,6 in GCSE Double Award Science. Selectors will also check that any specific entry requirements in terms of A-level subjects can be fulfilled.

Offers are normally made on the basis of 3 A-levels. Applicants repeating A-levels require BBC at the first attempt. Applicants are not normally asked to attend for interview.

Applicants offering two A-levels and one BTEC Subsidiary Diploma/National Extended Certificate (or equivalent qualification) will also be considered. Offers will be made in terms of the overall BTEC grade awarded. Please note that a maximum of one BTEC Subsidiary Diploma/National Extended Certificate (or equivalent) will be counted as part of an applicant’s portfolio of qualifications. The normal GCSE profile will be expected.

For applicants offering the Irish Leaving Certificate, please note that performance at Irish Junior Certificate (IJC) is taken into account. For last year’s entry, applicants for this degree must have had a minimum of six IJC grades at B/Higher Merit. The Selector also checks that any specific entry requirements in terms of Leaving Certificate subjects can be satisfied.

Applicants offering BTEC Extended Diplomas/National Extended Diplomas, Higher National Certificates and Higher National Diplomas are not normally considered for MEng entry but, if eligible, will be made a change course offer for the corresponding BEng programme.

Access course qualifications are not considered for entry to the MEng degree and applicants should apply for the corresponding BEng programme.

Subject to satisfactory academic performance during the first two years of the BEng course, it may be possible for students to transfer to the MEng programme at the end of Stage 2.

The information provided in the personal statement section and the academic reference together with predicted grades are noted but these are not the final deciding factors in whether or not a conditional offer can be made. However, they may be reconsidered in a tie break situation in August.

A-level General Studies and A-level Critical Thinking are not normally considered as part of a three A-level offer and, although they may be excluded where an applicant is taking 4 A-level subjects, the grade achieved could be taken into account if necessary in August/September.

If you are made an offer then you may be invited to a Faculty/School Open Day, which is usually held during the second semester. This will allow you the opportunity to visit the University and to find out more about the degree programme of your choice and the facilities on offer. It also gives you a flavour of the academic and social life at Queen's.

If you cannot find the information you need here, please contact the University Admissions and Access Service (admissions@qub.ac.uk), giving full details of your qualifications and educational background.

International Students

Our country/region pages include information on entry requirements, tuition fees, scholarships, student profiles, upcoming events and contacts for your country/region. Use the dropdown list below for specific information for your country/region.

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English Language Requirements

An IELTS score of 6.0 with a minimum of 5.5 in each test component or an equivalent acceptable qualification, details of which are available at: http://go.qub.ac.uk/EnglishLanguageReqs

Career Prospects

Introduction

Studying for a Chemical Engineering degree at Queen’s will provide you with the skills and employment-related experiences that are valued by employers, professional organisations and academic institutions. Graduates holding a degree from Queen’s are highly regarded by many local, national and international employers and many of our students are successful in securing employment in globally recognised industries well before graduation.
Chemical Engineering is a practical and useful degree which enables you to seek employment in a range of sectors including the pharmaceutical, energy, manufacturing and food industries. The opportunities widen further to sectors such as finance, business and research and many of our graduates embark on further study in specialised areas which align with their career aspirations.
We regularly consult and develop links with a large number of employers and have an industrial advisory board to advise the school on developments within the sector so that we can continually revise and update our courses to match industry demand.

Other Career-related information:

Queen’s is a member of the Russell Group and, therefore, one of the 20 universities most-targeted by leading graduate employers. Queen’s students will be advised and guided about career choice and, through the Degree Plus initiative, will have an opportunity to seek accreditation for skills development and experience gained through the wide range of extra-curricular activities on offer. See Queen’s University Belfast full Employability Statement for further information.

Degree Plus and other related initiatives: Recognising student diversity, as well as promoting employability enhancements and other interests, is part of the developmental experience at Queen’s. Students are encouraged to plan and build their own, personal skill and experiential profile through a range of activities including; recognised Queen’s Certificates, placements and other work experiences (at home or overseas), Erasmus study options elsewhere in Europe, learning development opportunities and involvement in wider university life through activities, such as clubs, societies, and sports.

Queen’s actively encourages this type of activity by offering students an additional qualification, the Degree Plus Award (and the related Researcher Plus Award for PhD and MPhil students). Degree Plus accredits wider experiential and skill development gained through extra-curricular activities that promote the enhancement of academic, career management, personal and employability skills in a variety of contexts. As part of the Award, students are also trained on how to reflect on the experience(s) and make the link between academic achievement, extracurricular activities, transferable skills and graduate employment. Participating students will also be trained in how to reflect on their skills and experiences and can gain an understanding of how to articulate the significance of these to others, e.g. employers.

Overall, these initiatives, and Degree Plus in particular, reward the energy, drive, determination and enthusiasm shown by students engaging in activities over-and-above the requirements of their academic studies. These qualities are amongst those valued highly by graduate employers

Employment Links

Our past students have also gained work placement with organisations including:
Invista, BP Chemicals, Shell, ExxonMobil, Almac, P&G, Pfizer, Merck Sharp & Dohme, WuXi, Eli-Lilly, GSK, Alexion, Seagate, Intel, Unilever, EDF and Norbrook.
Many research projects within the School have industrial input and are in collaboration with a wide variety of companies operating in the chemical sector. Given the close working relationships between industry and the School of Chemistry and Chemical Engineering, new opportunities to expand placements, industrial contact and career opportunities are continually developing.

Degree Plus/Future Ready Award for extra-curricular skills

In addition to your degree programme, at Queen's you can have the opportunity to gain wider life, academic and employability skills. For example, placements, voluntary work, clubs, societies, sports and lots more. So not only do you graduate with a degree recognised from a world leading university, you'll have practical national and international experience plus a wider exposure to life overall. We call this Degree Plus/Future Ready Award. It's what makes studying at Queen's University Belfast special.

Tuition Fees

Northern Ireland (NI) 1	£4,855
Republic of Ireland (ROI) 2	£4,855
England, Scotland or Wales (GB) 1	£9,535
EU Other 3	£25,300
International	£25,300

¹EU citizens in the EU Settlement Scheme, with settled status, will be charged the NI or GB tuition fee based on where they are ordinarily resident. Students who are ROI nationals resident in GB will be charged the GB fee.

² EU students who are ROI nationals resident in ROI are eligible for NI tuition fees.

³ EU Other students (excludes Republic of Ireland nationals living in GB, NI or ROI) are charged tuition fees in line with international fees.

The tuition fees quoted above for NI and ROI are the 2024/25 fees and will be updated when the new fees are known. In addition, all tuition fees will be subject to an annual inflationary increase in each year of the course. Fees quoted relate to a single year of study unless explicitly stated otherwise.

Tuition fee rates are calculated based on a student’s tuition fee status and generally increase annually by inflation. How tuition fees are determined is set out in the Student Finance Framework.

Additional course costs

Students are required to buy a laboratory coat and safety glasses in year 1 at a cost of approx. £20.

All Students

Depending on the programme of study, there may be extra costs which are not covered by tuition fees, which students will need to consider when planning their studies.

Students can borrow books and access online learning resources from any Queen's library. If students wish to purchase recommended texts, rather than borrow them from the University Library, prices per text can range from £30 to £100. Students should also budget between £30 to £75 per year for photocopying, memory sticks and printing charges.

Students undertaking a period of work placement or study abroad, as either a compulsory or optional part of their programme, should be aware that they will have to fund additional travel and living costs.

If a programme includes a major project or dissertation, there may be costs associated with transport, accommodation and/or materials. The amount will depend on the project chosen. There may also be additional costs for printing and binding.

Students may wish to consider purchasing an electronic device; costs will vary depending on the specification of the model chosen.

There are also additional charges for graduation ceremonies, examination resits and library fines.

Scholarships

Each year, we offer a range of scholarships and prizes for new students. Information on scholarships available.

How to Apply

Application for admission to full-time undergraduate and sandwich courses at the University should normally be made through the Universities and Colleges Admissions Service (UCAS). Full information can be obtained from the UCAS website at: www.ucas.com/students.

When to Apply

UCAS will start processing applications for entry in autumn 2025 from early September 2024.

The advisory closing date for the receipt of applications for entry in 2025 is still to be confirmed by UCAS but is normally in late January (18:00). This is the 'equal consideration' deadline for this course.

Applications from UK and EU (Republic of Ireland) students after this date are, in practice, considered by Queen’s for entry to this course throughout the remainder of the application cycle (30 June 2025) subject to the availability of places. If you apply for 2025 entry after this deadline, you will automatically be entered into Clearing.

Applications from International and EU (Other) students are normally considered by Queen's for entry to this course until 30 June 2025. If you apply for 2025 entry after this deadline, you will automatically be entered into Clearing.

Applicants are encouraged to apply as early as is consistent with having made a careful and considered choice of institutions and courses.

The Institution code name for Queen's is QBELF and the institution code is Q75.

Further information on applying to study at Queen's is available at: www.qub.ac.uk/Study/Undergraduate/How-to-apply/

Apply via UCAS

Terms and Conditions

The terms and conditions that apply when you accept an offer of a place at the University on a taught programme of study. Queen's University Belfast Terms and Conditions.

Additional Information for International (non-EU) Students

1. Applying through UCAS
   Most students make their applications through UCAS (Universities and Colleges Admissions Service) for full-time undergraduate degree programmes at Queen's. The UCAS application deadline for international students is 30 June 2025.
2. Applying direct
   The Direct Entry Application form is to be used by international applicants who wish to apply directly, and only, to Queen's or who have been asked to provide information in advance of submitting a formal UCAS application. Find out more.
3. Applying through agents and partners
   The University’s in-country representatives can assist you to submit a UCAS application or a direct application. Please consult the Agent List to find an agent in your country who will help you with your application to Queen’s University.

Download Undergraduate Prospectus